Administracja Centralna Uczelni - Wymiana międzynarodowa (S2)
Sylabus przedmiotu Instrumental analysis:
Informacje podstawowe
| Kierunek studiów | Wymiana międzynarodowa | ||
|---|---|---|---|
| Forma studiów | studia stacjonarne | Poziom | drugiego stopnia |
| Tytuł zawodowy absolwenta | |||
| Obszary studiów | — | ||
| Profil | |||
| Moduł | — | ||
| Przedmiot | Instrumental analysis | ||
| Specjalność | przedmiot wspólny | ||
| Jednostka prowadząca | Katedra Chemii Organicznej i Chemii Fizycznej | ||
| Nauczyciel odpowiedzialny | Elwira Wróblewska <Elwira.Wroblewska@zut.edu.pl> | ||
| Inni nauczyciele | Marta Sawicka <Marta.Sawicka@zut.edu.pl>, Elwira Wróblewska <Elwira.Wroblewska@zut.edu.pl> | ||
| ECTS (planowane) | 4,0 | ECTS (formy) | 4,0 |
| Forma zaliczenia | zaliczenie | Język | angielski |
| Blok obieralny | — | Grupa obieralna | — |
Formy dydaktyczne
Wymagania wstępne
| KOD | Wymaganie wstępne |
|---|---|
| W-1 | Basis of physical chemistry, organic chemistry, general chemistry, analytical methods. |
Cele przedmiotu
| KOD | Cel modułu/przedmiotu |
|---|---|
| C-1 | Theoretical and practical learning about instrumental methods applied in quantitative and qualitative analysis; |
| C-2 | Theoretical studies about the phenomena used in the particular method as well as practical interpretation of the results given. |
Treści programowe z podziałem na formy zajęć
| KOD | Treść programowa | Godziny |
|---|---|---|
| ćwiczenia audytoryjne | ||
| T-A-1 | The ways of preparing of the solution with a given concentration. | 2 |
| T-A-2 | The ways of expression of the content od some components of the solution. | 2 |
| T-A-3 | Units usually used in absorption spectra. | 1 |
| T-A-4 | The application of Lambert-Beer's low in quantitative analysis of single and multicomponent mixtures. | 4 |
| T-A-5 | Calibration curve and their application in quantitative analysis. | 1 |
| T-A-6 | The characteristic of the analytical method (limit of detection, method sensitivity and precision). | 1 |
| T-A-7 | The use of NMR spectroscopy in qualitative and quantitative analysis of organic compounds. | 2 |
| T-A-8 | The use of some information which are read off from chromatogram into qualitative and quantitative analysis of organic compounds | 2 |
| 15 | ||
| laboratoria | ||
| T-L-1 | Measurements of UV-vis spectra and their application in the studies of solute-solvent intermolecular interaction , as well as in quantitative analysis. | 10 |
| T-L-2 | The interpretation of HNMR spectra as a key to the determination of the structure of organic compounds. | 10 |
| T-L-3 | The application of IR method in qualitative and quantitative analysis of organic compounds. | 10 |
| T-L-4 | The application of chromatographic method in qualitative and quantitative analysis of multicomponent mixtures. | 10 |
| T-L-5 | The determination of some metals with the use of ASA method. | 5 |
| 45 | ||
| wykłady | ||
| T-W-1 | The fundamental definitions concerning analytical process, the kind of analytical method with respect to instrumental method analysis. | 1 |
| T-W-2 | Classification of the methods of instrumental analysis, particularly spectroscopic and chromatographic ones. | 1 |
| T-W-3 | Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties. | 1 |
| T-W-4 | Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation and their application in particular methods i.e. ultraviolet-visual spectroscopy (UV-VIS), infrared spectroscopy (IR), nuclear magnetic resonance spectroscopy (NMR), mass spectroscopy (MS), atomic absorption spectroscopy (AAS), X-ray absorption, atomic emission spectroscopy (AES), flame photometry, inductively coupled plasma spectrometry (ICP), X-ray fluorescence (XRF), atomic fluorescence. | 9 |
| T-W-5 | Explanation of phenomena, concepts, and definitions used in chromatographic methods. The ways of separation of a mixture components. | 3 |
| 15 | ||
Obciążenie pracą studenta - formy aktywności
| KOD | Forma aktywności | Godziny |
|---|---|---|
| ćwiczenia audytoryjne | ||
| A-A-1 | The participation in the classes. | 15 |
| A-A-2 | The individual preparation of student for the classes. | 15 |
| 30 | ||
| laboratoria | ||
| A-L-1 | The participation in the laboratory. | 45 |
| A-L-2 | The individual preparation of student for the laboratory. | 10 |
| A-L-3 | The preparation of laboratory report. | 5 |
| 60 | ||
| wykłady | ||
| A-W-1 | The participation in the lectures with the possibility of the discussion. | 15 |
| A-W-2 | Individual studies of the subject - reading of the recomended literature. | 10 |
| A-W-3 | The individual preparation of student for the exam. | 5 |
| 30 | ||
Metody nauczania / narzędzia dydaktyczne
| KOD | Metoda nauczania / narzędzie dydaktyczne |
|---|---|
| M-1 | The lectures with the discussion. |
| M-2 | Classes |
| M-3 | Laboratory |
Sposoby oceny
| KOD | Sposób oceny |
|---|---|
| S-1 | Ocena podsumowująca: Written exam and/or oral discussion. |
| S-2 | Ocena formująca: Assessment of laboratory written report. |
| S-3 | Ocena formująca: Assessment of homework assignments. |
| S-4 | Ocena formująca: Evaluation of the student’s work based on the student activity during the course. |
Zamierzone efekty kształcenia - wiedza
| Zamierzone efekty kształcenia | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|
| WM-WTiICh_2-_null_W01 Student knows the phenomena applied in the instrumental analysis. | — | — | C-1, C-2 | T-W-1, T-W-2, T-W-3, T-W-4, T-W-5 | M-1 | S-1 |
| WM-WTiICh_2-_null_W02 He has a knowledge about the fundamentals of the selected spectroscopic and chromatographic methods. | — | — | C-1, C-2 | T-W-3, T-W-4, T-W-5 | M-1 | S-1 |
Zamierzone efekty kształcenia - umiejętności
| Zamierzone efekty kształcenia | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|
| WM-WTiICh_2-_null_U01 Student is able to plan and carry out the experiment with the interpretation of obtained results. | — | — | C-1, C-2 | T-A-1, T-A-2, T-A-3, T-A-4, T-A-5, T-A-6, T-A-7, T-A-8, T-L-1, T-L-2, T-L-3, T-L-4, T-L-5 | M-2, M-3 | S-2, S-3, S-4 |
Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne
| Zamierzone efekty kształcenia | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|
| WM-WTiICh_2-_null_K01 Student is able to choose the appropriate method in order to solve particular problem concerning qualitative and/or quantitative analysis | — | — | C-1 | T-L-1, T-L-2, T-L-3, T-L-4, T-L-5, T-W-4, T-W-5 | M-1, M-3 | S-4 |
Kryterium oceny - wiedza
| Efekt kształcenia | Ocena | Kryterium oceny |
|---|---|---|
| WM-WTiICh_2-_null_W01 Student knows the phenomena applied in the instrumental analysis. | 2,0 | |
| 3,0 | Student knows the fundamentals of phenomena applied in the instrumental analysis. | |
| 3,5 | ||
| 4,0 | ||
| 4,5 | ||
| 5,0 | ||
| WM-WTiICh_2-_null_W02 He has a knowledge about the fundamentals of the selected spectroscopic and chromatographic methods. | 2,0 | |
| 3,0 | He has a knowledge about the fundamentals of a few methods of instrumental inanalysis. | |
| 3,5 | ||
| 4,0 | ||
| 4,5 | ||
| 5,0 |
Kryterium oceny - umiejętności
| Efekt kształcenia | Ocena | Kryterium oceny |
|---|---|---|
| WM-WTiICh_2-_null_U01 Student is able to plan and carry out the experiment with the interpretation of obtained results. | 2,0 | |
| 3,0 | Student is able to carry out the experiment with the simple interpretation of obtained results. | |
| 3,5 | ||
| 4,0 | ||
| 4,5 | ||
| 5,0 |
Kryterium oceny - inne kompetencje społeczne i personalne
| Efekt kształcenia | Ocena | Kryterium oceny |
|---|---|---|
| WM-WTiICh_2-_null_K01 Student is able to choose the appropriate method in order to solve particular problem concerning qualitative and/or quantitative analysis | 2,0 | |
| 3,0 | Student is able to choose the appropriate method in order to solve the problem concerning quantitative analysis. | |
| 3,5 | ||
| 4,0 | ||
| 4,5 | ||
| 5,0 |
Literatura podstawowa
- J. M. Hollas, Modern spectroscopy, John Wiley, 2004
- L.D. Field, S. Sternhall, J.R. Kalman, Organic structures from spectra, 3rd ed., Chichester, John Wiley and Son, 2002
- J.R. Chapman, Practical Organic Mass Spectrometry, 2nd ed., Chichester, John Wiley and Son, 1993
- Ira N. Levin, Molecular spectroscopy, Wiley-Interscience, New York, 1975
- C. N. R. Rao, Ultra-violet and visible spectroscopy: chemical applications, 3rd ed., Butterworths, London, 1975
- ed. D. A. Ramsay, Spectroscopy, University Park Press, London: Butterworths; Baltimore, 1976
- Stefan Hüfner, Photoelectron spectroscopy: principles and applications, 2nd ed., Springer, Berlin, 1996
Literatura dodatkowa
- Ch. Reichardt, Solvents and solvent effects in organic chemistry, 2nd rev. and enl. ed., Weinheim, VCH, 1990
- Pradip K. Ghosh, Introduction to photoelectron spectroscopy, John Wiley and Sons, New York, 1983
- M. Slavin, Atomic absorption spectroscopy, John Wiley & Sons, New York, 1978
- J. Mika, T. Török, Analytical emission spectroscopy : fundamentals, Akadémiai Kiadó, Budapest, 1973
- Yoshito Takeuchi and Alan P. Marchand, Applications of NMR spectroscopy to problems in stereochemistry and conformational analysis, Verlag Chemie International, Deerfield Beach, Florida, 1986