Administracja Centralna Uczelni - Wymiana międzynarodowa (S2)
Sylabus przedmiotu Spectroscopic methods:
Informacje podstawowe
| Kierunek studiów | Wymiana międzynarodowa | ||
|---|---|---|---|
| Forma studiów | studia stacjonarne | Poziom | drugiego stopnia |
| Tytuł zawodowy absolwenta | |||
| Obszary studiów | — | ||
| Profil | |||
| Moduł | — | ||
| Przedmiot | Spectroscopic methods | ||
| Specjalność | przedmiot wspólny | ||
| Jednostka prowadząca | Katedra Chemii Organicznej i Chemii Fizycznej | ||
| Nauczyciel odpowiedzialny | Marta Sawicka <Marta.Sawicka@zut.edu.pl> | ||
| Inni nauczyciele | Marta Sawicka <Marta.Sawicka@zut.edu.pl>, Elwira Wróblewska <Elwira.Wroblewska@zut.edu.pl> | ||
| ECTS (planowane) | 4,0 | ECTS (formy) | 4,0 |
| Forma zaliczenia | zaliczenie | Język | angielski |
| Blok obieralny | — | Grupa obieralna | — |
Formy dydaktyczne
Wymagania wstępne
| KOD | Wymaganie wstępne |
|---|---|
| W-1 | Fundamentals of physical chemistry. |
| W-2 | Fundamentals of organic chemistry. |
Cele przedmiotu
| KOD | Cel modułu/przedmiotu |
|---|---|
| C-1 | To gain the knowledge about the theory of spectroscopic methods and their application in qualitative and quantitative analysis. |
Treści programowe z podziałem na formy zajęć
| KOD | Treść programowa | Godziny |
|---|---|---|
| ćwiczenia audytoryjne | ||
| T-A-1 | Calculation of a compound concentration expressed in various concentration units. | 2 |
| T-A-2 | Calculation the concentration of a solution after dillution. | 2 |
| T-A-3 | Solving some excercisses concerning the interaction of the matter with light (absorbance, transmitance). | 1 |
| T-A-4 | Determination of compounds based on Lambert-Beer's low in single and multicomponent mixtures. | 3 |
| T-A-5 | The application of calibration curve in quantitative analysis of componds. | 2 |
| T-A-6 | Limit of detection, method sensitivity and precision - calculation. | 1 |
| T-A-7 | The application of NMR spectroscopy in qualitative and quantitative analysis of organic compounds (the calculation of the position of the band corresponding to particular proton on the basis on empirical equations, determination of a compound purity). | 2 |
| T-A-8 | Application of MS spectra in determination of organic compounds composition (Beynon table). | 2 |
| 15 | ||
| laboratoria | ||
| T-L-1 | The measurements of UV-vis spectra and their application in qualitative and quantitative analysis of various compounds. | 10 |
| T-L-2 | The recording and interpretation of IR spectra. | 10 |
| T-L-3 | Analysis of multicomponent mixtures by spectroscopic methods supported by computer programs. | 10 |
| T-L-4 | Precise analysis of NMR spectra with the use of technical software. | 10 |
| T-L-5 | The interpretation of MS spectra of various group of organic compounds. | 5 |
| 45 | ||
| wykłady | ||
| T-W-1 | Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties. Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation. | 2 |
| T-W-2 | The theory of ultraviolet-visual spectroscopy (UV-VIS); the Lambert-Beer's low and the reason of the departure from this low: association, solvatochromism, thermochromism, photochromism, halochromism. | 2 |
| T-W-3 | The application of UV-vis spectrophotometry to the analysis of multicomponent mixtures (theory, mathematics and software). | 2 |
| T-W-4 | The use of UV-vis spectrophotometers into the studies of luminescent materials. | 1 |
| T-W-5 | Infrared spectroscopy (IR) and its application to qualitative analysis of solids and liquids. | 2 |
| T-W-6 | The application of IR spectroscopy to quantitative analysis of compounds (methods, their possibilities and limitations). | 2 |
| T-W-7 | The theory of NMR spectrometry. The analysis of the spectra of various compounds. | 2 |
| T-W-8 | MS spectrometry: types of MS spectrometers, the methods of ionisation. | 2 |
| 15 | ||
Obciążenie pracą studenta - formy aktywności
| KOD | Forma aktywności | Godziny |
|---|---|---|
| ćwiczenia audytoryjne | ||
| A-A-1 | The participation in the classes. | 15 |
| A-A-2 | The individual preparation of student for the classes. | 15 |
| 30 | ||
| laboratoria | ||
| A-L-1 | The participation in the laboratory. | 45 |
| A-L-2 | The individual preparation of student for the laboratory. | 15 |
| 60 | ||
| wykłady | ||
| A-W-1 | The participation in the lectures with the possibility of the discussion. | 15 |
| A-W-2 | Individual studies of the subject - reading of the recomended literature. | 10 |
| A-W-3 | Individual analysis of avialable spectra | 5 |
| 30 | ||
Metody nauczania / narzędzia dydaktyczne
| KOD | Metoda nauczania / narzędzie dydaktyczne |
|---|---|
| M-1 | The lectures with the discussion. |
| M-2 | Classes |
| M-3 | Laboratory |
Sposoby oceny
| KOD | Sposób oceny |
|---|---|
| S-1 | Ocena podsumowująca: Written exam and/or oral discussion |
| S-2 | Ocena formująca: Assessment of laboratory written report |
| S-3 | Ocena formująca: Assessment of homework assignments. |
| S-4 | Ocena formująca: Evaluation of the student’s work based on the student activity during the course. |
Zamierzone efekty kształcenia - wiedza
| Zamierzone efekty kształcenia | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|
| WM-WTiICh_2-_null_W01 He has a knowledge about the fundamentals of the selected spectroscopic method and their application in qualitative and quantitative analysis. | — | — | C-1 | T-W-1, T-W-2, T-W-3, T-W-4, T-W-5, T-W-6, T-W-7, T-W-8 | M-1 | S-1, S-4 |
Zamierzone efekty kształcenia - umiejętności
| Zamierzone efekty kształcenia | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|
| WM-WTiICh_2-_null_U01 Student is able to make some calculation concerning the analysis with the interpretation of obtained results. | — | — | C-1 | T-A-1, T-A-2, T-A-3, T-A-4, T-A-5, T-A-6, T-A-7, T-A-8 | M-2, M-3 | S-2, S-3 |
| WM-WTiICh_2-_null_U02 Student can plane and carry the experiment with the interpretation of obtained results. | — | — | C-1 | T-L-1, T-L-2, T-L-3, T-L-4, T-L-5 | M-3 | S-2, S-4 |
Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne
| Zamierzone efekty kształcenia | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|
| WM-WTiICh_2-_null_K01 Student is able to choose the appropriate method in order to solve particular problem. | — | — | C-1 | T-L-1, T-L-2, T-L-3, T-L-4, T-L-5, T-W-1 | M-3 | S-4 |
Kryterium oceny - wiedza
| Efekt kształcenia | Ocena | Kryterium oceny |
|---|---|---|
| WM-WTiICh_2-_null_W01 He has a knowledge about the fundamentals of the selected spectroscopic method and their application in qualitative and quantitative analysis. | 2,0 | |
| 3,0 | Student has a fundamental knowledge about particular spectroscopic method. | |
| 3,5 | ||
| 4,0 | ||
| 4,5 | ||
| 5,0 |
Kryterium oceny - umiejętności
| Efekt kształcenia | Ocena | Kryterium oceny |
|---|---|---|
| WM-WTiICh_2-_null_U01 Student is able to make some calculation concerning the analysis with the interpretation of obtained results. | 2,0 | |
| 3,0 | Student is able to make some calculation concerning the analysis. | |
| 3,5 | ||
| 4,0 | ||
| 4,5 | ||
| 5,0 | ||
| WM-WTiICh_2-_null_U02 Student can plane and carry the experiment with the interpretation of obtained results. | 2,0 | |
| 3,0 | Student can carry simple experiment with the interpretation of obtained results. | |
| 3,5 | ||
| 4,0 | ||
| 4,5 | ||
| 5,0 |
Kryterium oceny - inne kompetencje społeczne i personalne
| Efekt kształcenia | Ocena | Kryterium oceny |
|---|---|---|
| WM-WTiICh_2-_null_K01 Student is able to choose the appropriate method in order to solve particular problem. | 2,0 | |
| 3,0 | Student is able to choose the appropriate method in order to solve less complicated problem. | |
| 3,5 | ||
| 4,0 | ||
| 4,5 | ||
| 5,0 |
Literatura podstawowa
- Field, L. D, Strnhell, S, Kalman, J.R., Organic structures from spectra, Chichester: John Wiley and Sons, 2002
- Bartecki, A. , Lang, L., Absorption spectra in the ultraviolet and visible region., House of the Hungarian. Academy of Sciences, Budapest, 1982
- Láng, L., Holly, S, Sohár, P., Absorption spectra in the infrared region, Akadémiai Kiadó, Budapest, 1980
- Rahman, Atta-ur, One and two dimensional NMR spectroscopy, Elsevier, Amsterdam, 2011
- Perkampus, Heinz-Helmut, Encyclopedia of spectroscopy, Weinheim : VCH, 1995
Literatura dodatkowa
- Reichardt, Christian, Solvents and solvent effects in organic chemistry, Weinheim : VCH, 1990
- Evans, Myron Wyn, S., The photon’s magnetic field : optical NMR spectroscopy, World Scientific, Singapore, 1992
- Strobel, Howard A., Chemical instrumentation : a systematic approach to instrumental analysis, Reading, Mass. : Addison-Wesley, 2011