Administracja Centralna Uczelni - Wymiana międzynarodowa (S2)
Sylabus przedmiotu Instrumental analysis in chemical engineering:
Informacje podstawowe
| Kierunek studiów | Wymiana międzynarodowa | ||
|---|---|---|---|
| Forma studiów | studia stacjonarne | Poziom | drugiego stopnia |
| Tytuł zawodowy absolwenta | |||
| Obszary studiów | — | ||
| Profil | |||
| Moduł | — | ||
| Przedmiot | Instrumental analysis in chemical engineering | ||
| Specjalność | przedmiot wspólny | ||
| Jednostka prowadząca | Katedra Chemii Nieorganicznej i Analitycznej | ||
| Nauczyciel odpowiedzialny | Piotr Tabero <Piotr.Tabero@zut.edu.pl> | ||
| Inni nauczyciele | Monika Bosacka <Monika.Bosacka@zut.edu.pl>, Anna Błońska-Tabero <Anna.Blonska-Tabero@zut.edu.pl>, Grażyna Dąbrowska <Grazyna.Dabrowska@zut.edu.pl>, Elżbieta Filipek <Elzbieta.Filipek@zut.edu.pl>, Piotr Tabero <Piotr.Tabero@zut.edu.pl>, Elżbieta Tomaszewicz <Elzbieta.Tomaszewicz@zut.edu.pl> | ||
| ECTS (planowane) | 4,0 | ECTS (formy) | 4,0 |
| Forma zaliczenia | zaliczenie | Język | polski |
| Blok obieralny | — | Grupa obieralna | — |
Formy dydaktyczne
Wymagania wstępne
| KOD | Wymaganie wstępne |
|---|---|
| W-1 | Fundamentals of mathematics, physics and chemistry |
Cele przedmiotu
| KOD | Cel modułu/przedmiotu |
|---|---|
| C-1 | To acqaint students with the selected instrumental methods frequently applied in industry and laboratories for identification of raw materials and products as well as for determination of their crucial properties. |
| C-2 | To teach students how to choose proper analytical method to obtain certain research goal. |
| C-3 | To teach students how to use data gained from measurements, available data bases and literature |
Treści programowe z podziałem na formy zajęć
| KOD | Treść programowa | Godziny |
|---|---|---|
| ćwiczenia audytoryjne | ||
| T-A-1 | Sieve analysis. Standards. Sieving with test sieves. Microscopic determination of size and shape of grains. Microscopic inspection of quality of test sieves. Metallographic inspection of alloys. | 4 |
| T-A-2 | Definition of crystalline solid. Morphology of crystals. Analysis and description of crystal, single crystal, twinns, policrystalline substance, amorphous substance, gravel, sand, silt, mineral and rock. Powder X-ray diffraction. X-ray phase analysis. Identification of metals and alloys. Identyfication of minerals, and components of rocks and sands from different locations. | 4 |
| T-A-3 | Indexation of powder diffraction patterns. Determination of lattice parameters. Measurement of density using pycnometric and buoyancy methods. Rentgenographic density. | 4 |
| T-A-4 | XRD quantitative phase analysis. Determination of grain size and lattice distortions. | 4 |
| T-A-5 | High-temperature XRD measurements. Determination of coefficients of thermal expansion. Anisotrophy of thermal expansion. Investigations of polymorphic phase transitions. | 2 |
| T-A-6 | Thermal analysis. Identyfication and characterization of raw materials and products of chemical industry by using DTA-TGA methods. Determination of coefficients of thermal expansion by using dilatometric method. Determiantion of thermal stability of substances and sorption properties of molecular sieves. | 4 |
| T-A-7 | Application of IR, NIR and UV-Vis methods for identification of substances and coordination polyhedra building of their structures. Detection of small amounts of contaminants and ions with the help of UV-Vis and AAS. | 4 |
| T-A-8 | Identification and determination of properties of precious metals and precious stones by using XRD, IR, NIR, UV-Vis and density measurements. Identification of counterfeit coins and simulants of precious stones. | 4 |
| 30 | ||
| wykłady | ||
| T-W-1 | What are the instrumental analytical methods ? Classification of analytical methods.Choosing an analytical method. | 2 |
| T-W-2 | Physical properties of substances. Measurements of density of solids and liquids. | 2 |
| T-W-3 | Optical microscopy versus electron microscopy. Microscope solutions for metallography. | 2 |
| T-W-4 | Crystal, single crystal, gravel, sand, silt. Grain size and shape measurement methods. Sieve analysis. | 2 |
| T-W-5 | X-rays and their properties. X-ray fluorescence spectroscopy XRF . | 2 |
| T-W-6 | X-ray diffraction XRD and powder X-ray diffraction. X-ray qualitative phase analysis. | 2 |
| T-W-7 | Indexation of powder diffraction patterns and determination of lattice parameters. Diffractometric method of grain size and lattice distortion determination. | 2 |
| T-W-8 | High-temperature, low-temperature and high-pressure rentgenographic measurements. Investigations of thermal expansion . | 2 |
| T-W-9 | Rengenographic investigations of metals and alloys, solid solutions, nanocrystaline, semicrystalline and amorphous materials. | 2 |
| T-W-10 | Thermal analyasis. DTA, TGA and DSC methods. | 2 |
| T-W-11 | Dilatometric measurements of thermal expansion. Determination of thermal stability of substances and sorption properties of molecular sieves. | 2 |
| T-W-12 | IR and NIR spectroscopic methods. Thermography. | 2 |
| T-W-13 | UV-Vis spectroscopy. IR, UV-Vis-NIR methods for identification of substances and detection of small amounts of contaminants. | 2 |
| T-W-14 | Atomic absorption spectrposcopy AAS. | 2 |
| T-W-15 | The final written exam. | 2 |
| 30 | ||
Obciążenie pracą studenta - formy aktywności
| KOD | Forma aktywności | Godziny |
|---|---|---|
| ćwiczenia audytoryjne | ||
| A-A-1 | Participation inworkshop | 30 |
| A-A-2 | Participation in consultations | 2 |
| A-A-3 | Self-study of literature | 16 |
| A-A-4 | Preparation of written reports | 12 |
| 60 | ||
| wykłady | ||
| A-W-1 | Participation in lectures | 28 |
| A-W-2 | Participation in consultations | 2 |
| A-W-3 | Self-study of literature | 14 |
| A-W-4 | Preparing to pass wrriten exam based on the indicated literature and other sources of knowledge | 14 |
| A-W-5 | Finnal written exam | 2 |
| 60 | ||
Metody nauczania / narzędzia dydaktyczne
| KOD | Metoda nauczania / narzędzie dydaktyczne |
|---|---|
| M-1 | Informative lecture with multimedia instruments, explanation |
| M-2 | Work with computers and and dedicated software. |
Sposoby oceny
| KOD | Sposób oceny |
|---|---|
| S-1 | Ocena formująca: Final written exam |
| S-2 | Ocena formująca: Written reports. |
Zamierzone efekty kształcenia - wiedza
| Zamierzone efekty kształcenia | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|
| WM-WTiICh_2-_??_W01 Student knows physical properties of substances and terminology associated with analytical methods. | — | — | — | — | — | — |
| WM-WTiICh_2-_??_W02 Student knows construction and operation techniques of equipment used for identification of substances and determination of their properties | — | — | — | — | — | — |
Zamierzone efekty kształcenia - umiejętności
| Zamierzone efekty kształcenia | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|
| WM-WTiICh_2-_??_U01 Student can choose proper research method to obtain a certain research goal | — | — | — | — | — | — |
| WM-WTiICh_2-_??_U02 Student knows how to explain the data obtained and the phenomena exhibited in the materials analysis, knows how to design studies and elaborate results | — | — | — | — | — | — |
Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne
| Zamierzone efekty kształcenia | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|
| WM-WTiICh_2-_??_K01 Student knows safety procedures for analytical equipment and understands importance of permanent learning to improve personal competencies | — | — | — | — | — | — |
Literatura podstawowa
- C. Giacovazzo, H. Z. Monaco, D. Biterbo, F. Scordari, G. Gilli, G. Zanotti, M. Catt, Fundamentals of Crystallography, IUCR, Oxford University Press, Oxford, 2000
- B. D. Cullity, Elements of X-ray Diffraction, Addison-Wesley Publishing Company, Inc., London, 1978
- A. Gaunier, X-ray Diffraction in Crystals, Imperfect Crystals, and Amorphous Bodies, Courier Corporation, New York, 1994
- A. AUTHIER, G. CHAPUIS, EDS, A LITTLE DICTIONARY OF CRYSTALLOGRAPHY, INTERNATIONAL UNION OF CRYSTALLOGRAPHY, 2017, 2ND EDITION
- D. A. Skoog, F. J. Holler, S. R. Crouch, Principles of Instrumental Analysis, Brooks Cole, 2006, 6-th Edition
- S. Petrozz, Practical Instrumental Analysis: Methods, Quality Assurance and Laboratory Management, Wiley, 2012
- M. Granger, Instrumental Analysis, Revised Edition, Revised Updated Edition, Oxford University Press, Oxford, 2013
- J. Śestak, Heat, Thermal Analysis and Society, Nukleus HK, Hradec Kralove, 2004
- P. Gabbott Ed., Principles and Applications of Thermal Analysis, Wiley, 2008
- S. Franca, L. M. L. Nollet, Spectroscopic methods In Food Analysis, CRC Press, 2018
Literatura dodatkowa
- International Union of Crystallography: https://www.iucr.org