Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Wydział Technologii i Inżynierii Chemicznej - Chemical Engineering (S2)
specjalność: Modern and Green Chemical Engineering

Sylabus przedmiotu Instrumental Analysis in Organic Chemical Engineering:

Informacje podstawowe

Kierunek studiów Chemical Engineering
Forma studiów studia stacjonarne Poziom drugiego stopnia
Tytuł zawodowy absolwenta magister inżynier
Obszary studiów charakterystyki PRK, kompetencje inżynierskie PRK
Profil ogólnoakademicki
Moduł —
Przedmiot Instrumental Analysis in Organic Chemical Engineering
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Chemii Organicznej i Chemii Fizycznej
Nauczyciel odpowiedzialny Jacek Sośnicki <Jacek.Sosnicki@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 4,0 ECTS (formy) 4,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny — Grupa obieralna —

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
wykładyW1 30 2,00,50zaliczenie
laboratoriaL1 45 2,00,50zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Basic knowledge of organic chemistry.

Cele przedmiotu

KODCel modułu/przedmiotu
C-1Acquainting students with the fundamental chromatographic (GC, GC-MS, HPLC) and spectroscopic (UV-VIS, IR, NMR) methods and Mass Spectrometry, applied for analysis of organic compounds.
C-2Acquainting students with practical aspects of chromatographic analyses and selected spectral methods.
C-3Preparing students for standalone qualitative and quantitative analysis of organic compounds by chromatographic methods and for interpretation of measurement results obtained by UV-VIS, IR, MS and 1H, 13C NMR methods.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
laboratoria
T-L-1Practical application of chromatographic methods (GC, GC-MS, HPLC) in analysis of organic compounds and products. Sample preparation, quantitative and qualitative analysis, evaluation of results.20
T-L-2Practical application of IR, FTIR and UV-Vis methods in analysis of organic compounds.10
T-L-3Samples preparations, practical aspects of measurements and structural analysis of organic compounds by MS and 1H, 13C NMR methods.15
45
wykłady
T-W-1Chromatographic methods: Gas Chromatography (GC), High Performance Liquid Chromatography (HPLC). Instrumentation, application of different detectors. Optimization of analysis conditions. Quantitative and qualitative analysis. Method development and validation. Problems of trace analysis. Sources of measurements errors. Sample preparation techniques.10
T-W-2Spectroscopic methods: Infrared Spectroscopy (IR), Fourier Transform Infrared Spectroscopy (FTIR), Ultraviolet-Visible Spectroscopy (UV-Vis). Instrumentation, application, practical aspects and problems in analyses.5
T-W-3Overview of Mass Spectrometry (MS) and 1H, 13C Nuclear Magnetic Resonance (NMR) as fundamental methods for analysis of organic compounds. Instrumentation, method development, practical aspects and problems in analyses.14
T-W-4The final single choice test.1
30

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
laboratoria
A-L-1participation in laboratory classes45
A-L-2preparing labs reports5
50
wykłady
A-W-1attendance at lectures30
A-W-2individual study of literature8
A-W-3individual learning for the test10
A-W-4consultations2
50

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1powerpoint and whiteboard lectures
M-2laboratory exercises
M-3in-class discussion

Sposoby oceny

KODSposób oceny
S-1Ocena formująca: continuous assessment
S-2Ocena podsumowująca: evaluation of written reports
S-3Ocena podsumowująca: final writing test

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_B04_W01
The student has in-depth knowledge on instrumental methods of analyses of organic compounds (chromatography, FTIR, UV-VIS, NMR, MS).		ChEn_2A_W01——C-1, C-2, C-3T-W-3, T-L-3, T-W-1, T-W-2, T-L-1, T-L-2M-1, M-2, M-3S-1, S-2, S-3

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_B04_U01
The student demonstrates the ability to analyze chromatographic (GC, GCMS, HPLC) and spectroscopic data (IR, UV-VIS, NMR, MS) obtained for organic compounds.		ChEn_2A_U01, ChEn_2A_U05, ChEn_2A_U06, ChEn_2A_U08——C-2, C-3T-L-3, T-L-1, T-L-2M-2, M-3S-1, S-2

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_B04_K01
The student is aware of the importance of instrumental analysis in organic chemical engineering for impovement of the quality of life.		ChEn_2A_K02——C-1, C-2, C-3T-W-3, T-L-3, T-W-1, T-W-2, T-L-1, T-L-2M-1, M-3S-1, S-3

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_B04_W01
The student has in-depth knowledge on instrumental methods of analyses of organic compounds (chromatography, FTIR, UV-VIS, NMR, MS).		2,0
3,0student is able to demonstrate the knowledge related to important aspects of instrumental analysis of organic compounds (more than 55% correct answers in final test)
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_B04_U01
The student demonstrates the ability to analyze chromatographic (GC, GCMS, HPLC) and spectroscopic data (IR, UV-VIS, NMR, MS) obtained for organic compounds.		2,0
3,0student is able to perform analysis of chromatographic and spectroscopic data and prepare laboratory raports with the help of a teacher
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_B04_K01
The student is aware of the importance of instrumental analysis in organic chemical engineering for impovement of the quality of life.		2,0
3,0student understands the importance of instrumental analysis in organic chemical engineering and was committed enough to meet the basic requirements of the course
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. McNair H.M., Miller J.M., Basic Gas Chromatography, Wiley, 2009, II ed.
  2. Snyder L.R., Kirkland J.L., Dolan J.W., Introduction to Modern Liqiud Chromatography, Wiley, 2010
  3. Ian Fleming, Dudley Williams, Spectroscopic Methods in Organic Chemistry, Springer, 2019, 7th Edition, online access
  4. Edwin D. Becker., High resolution NMR : theory and chemical applications, Academic Press, San Diego, 2000
  5. Eberhard Breitmaier ; transl. by Julia Wade, Structure elucidation by NMR in organic chemistry : a practical guide, John Wiley & Sons, Chichester, 1993
  6. ed. Kenzo Hiraoka., Fundamentals of mass spectrometry, Springer, Springer, 2013

Literatura dodatkowa

  1. Peter R. Griffiths, James A. De Haseth, James D. Winefordner, Fourier Transform Infrared Spectrometry, WILEY, 2007, 2nd Edition

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Practical application of chromatographic methods (GC, GC-MS, HPLC) in analysis of organic compounds and products. Sample preparation, quantitative and qualitative analysis, evaluation of results.20
T-L-2Practical application of IR, FTIR and UV-Vis methods in analysis of organic compounds.10
T-L-3Samples preparations, practical aspects of measurements and structural analysis of organic compounds by MS and 1H, 13C NMR methods.15
45

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Chromatographic methods: Gas Chromatography (GC), High Performance Liquid Chromatography (HPLC). Instrumentation, application of different detectors. Optimization of analysis conditions. Quantitative and qualitative analysis. Method development and validation. Problems of trace analysis. Sources of measurements errors. Sample preparation techniques.10
T-W-2Spectroscopic methods: Infrared Spectroscopy (IR), Fourier Transform Infrared Spectroscopy (FTIR), Ultraviolet-Visible Spectroscopy (UV-Vis). Instrumentation, application, practical aspects and problems in analyses.5
T-W-3Overview of Mass Spectrometry (MS) and 1H, 13C Nuclear Magnetic Resonance (NMR) as fundamental methods for analysis of organic compounds. Instrumentation, method development, practical aspects and problems in analyses.14
T-W-4The final single choice test.1
30

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1participation in laboratory classes45
A-L-2preparing labs reports5
50
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1attendance at lectures30
A-W-2individual study of literature8
A-W-3individual learning for the test10
A-W-4consultations2
50
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_B04_W01The student has in-depth knowledge on instrumental methods of analyses of organic compounds (chromatography, FTIR, UV-VIS, NMR, MS).
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_W01Graduate has in-depth knowledge in the field of chemical processes, including appropriate selection of materials, raw materials, methods, techniques, equipment and devices for the implementation of chemical and biochemical processes and characterization of the raw materials and products obtained.
Cel przedmiotuC-1Acquainting students with the fundamental chromatographic (GC, GC-MS, HPLC) and spectroscopic (UV-VIS, IR, NMR) methods and Mass Spectrometry, applied for analysis of organic compounds.
C-2Acquainting students with practical aspects of chromatographic analyses and selected spectral methods.
C-3Preparing students for standalone qualitative and quantitative analysis of organic compounds by chromatographic methods and for interpretation of measurement results obtained by UV-VIS, IR, MS and 1H, 13C NMR methods.
Treści programoweT-W-3Overview of Mass Spectrometry (MS) and 1H, 13C Nuclear Magnetic Resonance (NMR) as fundamental methods for analysis of organic compounds. Instrumentation, method development, practical aspects and problems in analyses.
T-L-3Samples preparations, practical aspects of measurements and structural analysis of organic compounds by MS and 1H, 13C NMR methods.
T-W-1Chromatographic methods: Gas Chromatography (GC), High Performance Liquid Chromatography (HPLC). Instrumentation, application of different detectors. Optimization of analysis conditions. Quantitative and qualitative analysis. Method development and validation. Problems of trace analysis. Sources of measurements errors. Sample preparation techniques.
T-W-2Spectroscopic methods: Infrared Spectroscopy (IR), Fourier Transform Infrared Spectroscopy (FTIR), Ultraviolet-Visible Spectroscopy (UV-Vis). Instrumentation, application, practical aspects and problems in analyses.
T-L-1Practical application of chromatographic methods (GC, GC-MS, HPLC) in analysis of organic compounds and products. Sample preparation, quantitative and qualitative analysis, evaluation of results.
T-L-2Practical application of IR, FTIR and UV-Vis methods in analysis of organic compounds.
Metody nauczaniaM-1powerpoint and whiteboard lectures
M-2laboratory exercises
M-3in-class discussion
Sposób ocenyS-1Ocena formująca: continuous assessment
S-2Ocena podsumowująca: evaluation of written reports
S-3Ocena podsumowująca: final writing test
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student is able to demonstrate the knowledge related to important aspects of instrumental analysis of organic compounds (more than 55% correct answers in final test)
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_B04_U01The student demonstrates the ability to analyze chromatographic (GC, GCMS, HPLC) and spectroscopic data (IR, UV-VIS, NMR, MS) obtained for organic compounds.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_U01Graduate is able to utilize the in-depth knowledge in the field of chemical processes, including appropriate selection of materials, raw materials, methods, techniques, equipment and devices for the implementation of chemical and biochemical processes and characterization of the raw materials and products obtained.
ChEn_2A_U05Graduate is able to make and verify hypotheses related to simple research problems.
ChEn_2A_U06Graduate is able to analyse and solve complex problems related to chemical technology and process engineering on the basis of specialist knowledge, bibliographic resources, databases and other sources.
ChEn_2A_U08Graduate is able to apply the principles of occupational health and safety in the laboratory.
Cel przedmiotuC-2Acquainting students with practical aspects of chromatographic analyses and selected spectral methods.
C-3Preparing students for standalone qualitative and quantitative analysis of organic compounds by chromatographic methods and for interpretation of measurement results obtained by UV-VIS, IR, MS and 1H, 13C NMR methods.
Treści programoweT-L-3Samples preparations, practical aspects of measurements and structural analysis of organic compounds by MS and 1H, 13C NMR methods.
T-L-1Practical application of chromatographic methods (GC, GC-MS, HPLC) in analysis of organic compounds and products. Sample preparation, quantitative and qualitative analysis, evaluation of results.
T-L-2Practical application of IR, FTIR and UV-Vis methods in analysis of organic compounds.
Metody nauczaniaM-2laboratory exercises
M-3in-class discussion
Sposób ocenyS-1Ocena formująca: continuous assessment
S-2Ocena podsumowująca: evaluation of written reports
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student is able to perform analysis of chromatographic and spectroscopic data and prepare laboratory raports with the help of a teacher
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_B04_K01The student is aware of the importance of instrumental analysis in organic chemical engineering for impovement of the quality of life.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_K02Graduate is aware of the importance of knowledge in solving of cognitive and practical problems and is ready to consult experts in the case of difficult problems.
Cel przedmiotuC-1Acquainting students with the fundamental chromatographic (GC, GC-MS, HPLC) and spectroscopic (UV-VIS, IR, NMR) methods and Mass Spectrometry, applied for analysis of organic compounds.
C-2Acquainting students with practical aspects of chromatographic analyses and selected spectral methods.
C-3Preparing students for standalone qualitative and quantitative analysis of organic compounds by chromatographic methods and for interpretation of measurement results obtained by UV-VIS, IR, MS and 1H, 13C NMR methods.
Treści programoweT-W-3Overview of Mass Spectrometry (MS) and 1H, 13C Nuclear Magnetic Resonance (NMR) as fundamental methods for analysis of organic compounds. Instrumentation, method development, practical aspects and problems in analyses.
T-L-3Samples preparations, practical aspects of measurements and structural analysis of organic compounds by MS and 1H, 13C NMR methods.
T-W-1Chromatographic methods: Gas Chromatography (GC), High Performance Liquid Chromatography (HPLC). Instrumentation, application of different detectors. Optimization of analysis conditions. Quantitative and qualitative analysis. Method development and validation. Problems of trace analysis. Sources of measurements errors. Sample preparation techniques.
T-W-2Spectroscopic methods: Infrared Spectroscopy (IR), Fourier Transform Infrared Spectroscopy (FTIR), Ultraviolet-Visible Spectroscopy (UV-Vis). Instrumentation, application, practical aspects and problems in analyses.
T-L-1Practical application of chromatographic methods (GC, GC-MS, HPLC) in analysis of organic compounds and products. Sample preparation, quantitative and qualitative analysis, evaluation of results.
T-L-2Practical application of IR, FTIR and UV-Vis methods in analysis of organic compounds.
Metody nauczaniaM-1powerpoint and whiteboard lectures
M-3in-class discussion
Sposób ocenyS-1Ocena formująca: continuous assessment
S-3Ocena podsumowująca: final writing test
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student understands the importance of instrumental analysis in organic chemical engineering and was committed enough to meet the basic requirements of the course
3,5
4,0
4,5
5,0