Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Wydział Technologii i Inżynierii Chemicznej - Chemical Engineering (S2)

Sylabus przedmiotu Instrumental Analysis in Inorganic Chemical Engineering:

Informacje podstawowe

Kierunek studiów Chemical Engineering
Forma studiów studia stacjonarne Poziom drugiego stopnia
Tytuł zawodowy absolwenta magister inżynier
Obszary studiów charakterystyki PRK, kompetencje inżynierskie PRK
Profil ogólnoakademicki
Moduł —
Przedmiot Instrumental Analysis in Inorganic Chemical Engineering
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Technologii Chemicznej Nieorganicznej i Inżynierii Środowiska
Nauczyciel odpowiedzialny Joanna Grzechulska-Damszel <Joanna.Grzechulska@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 4,0 ECTS (formy) 4,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny — Grupa obieralna —

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
laboratoriaL1 45 2,00,50zaliczenie
wykładyW1 30 2,00,50zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Analytical chemistry

Cele przedmiotu

KODCel modułu/przedmiotu
C-1Student knows specified testing/analysis techniques of the basic parameters of inorganic products/materials

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
laboratoria
T-L-1Characterisation of catalytic materials10
T-L-2Characterisation of carbon materials10
T-L-3Characterisation of fertilizers5
T-L-4XRD as a tool for investigation of amorphous, semicrystaline and crystalline materials5
T-L-5Analysis of IR spectra of various groups of inorganic compounds.5
T-L-6Application of the DTA and TG methods for testing inorganic substances and their mixtures (thermal stability, temperature and way of melting, thermal decomposition mechanism etc.).5
T-L-7Analysis of NMR and CP MAS spectra of inorganic compounds. Case study.5
45
wykłady
T-W-1Methods of sampling and prepatation of samples for analysis2
T-W-2Application of specified methods/techniques for characterisation of inorganic products like catalysts, carbon materials and fertilizers, such as: XRF, XPS, SEM/EDX, BET, DLS, UVvis/DRS, ICP, elemental analysis (O, N, H, C, S)8
T-W-3Solving of the crystal structure2
T-W-4Rietveld refinement2
T-W-5XRD investigations of amorphous, semicrystaline and crystalline materials2
T-W-6Introduction to IR spectroscopy. Overview of instrumentation to use to study of inorganic compound. Applications in inorganic chemistry (merits and demerits).4
T-W-7Thermal analysis methods, their division and scope of applications. Selected measurement techniques: Differential thermal analysis (DTA) and thermogravimetry (TG). Physicochemical phenomena during thermal processing of solids. Recorded effects and their characteristic parameters.2
T-W-8Influence of measurement conditions (sample mass, particle size, gas atmosphere, heating rate, sample container shape) on the test result.2
T-W-9Quantitative and qualitative interpretation of DTA, TG results. Examples of special applications of thermal analysis methods for the determination of substance properties and the construction of phase diagrams.2
T-W-10NMR and CP MAS NMR of nuclei others than 1H and 13C. Equippments, practical applications and limitations.4
30

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
laboratoria
A-L-1Obligatory attendance at the classes45
A-L-2Preparation of the reports5
50
wykłady
A-W-1Attendance at the lectures30
A-W-2Individual literature studies10
A-W-3Preparation for the exam10
50

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Lecture
M-2Laboratory

Sposoby oceny

KODSposób oceny
S-1Ocena podsumowująca: Laboratory - attendance and reports
S-2Ocena podsumowująca: Lecture - exam

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_B05_W01
Student knows the methods of inorganic samples collecting and preparation for instrumental analysis. Student understands the basics of the analytical procedures and the criteria for for selection of particular techniques depending on the purpose of the analysis		ChEn_2A_W01——C-1T-W-10, T-L-7, T-W-3, T-W-4, T-W-5, T-L-4, T-W-1, T-W-2, T-L-1, T-L-2, T-L-3, T-W-6, T-L-5, T-L-6, T-W-7, T-W-8, T-W-9M-1, M-2S-1, S-2

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_B05_U01
Student can choose the method of sampling and preparing samples for secified analysis as well as choose the analytical method. Student is able to perform specified determinations and analysis.		ChEn_2A_U01——C-1T-W-10, T-L-7, T-W-3, T-W-4, T-W-5, T-L-4, T-W-1, T-W-2, T-L-1, T-L-2, T-L-3, T-W-6, T-L-5, T-L-6, T-W-7, T-W-8, T-W-9M-1, M-2S-1, S-2

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_B05_K01
Student can make the initial assesment and choose an analytical method/technique required for characterisation of particular material/product. Student is able to work in team to achive particular effect of characterisation of tested materials/products.		ChEn_2A_K02——C-1T-W-10, T-L-7, T-W-3, T-W-4, T-W-5, T-L-4, T-W-1, T-W-2, T-L-1, T-L-2, T-L-3, T-W-6, T-L-5, T-L-6, T-W-7, T-W-8, T-W-9M-1, M-2S-1, S-2

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_B05_W01
Student knows the methods of inorganic samples collecting and preparation for instrumental analysis. Student understands the basics of the analytical procedures and the criteria for for selection of particular techniques depending on the purpose of the analysis		2,0
3,0The student's knowledge is at the level of 60%
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_B05_U01
Student can choose the method of sampling and preparing samples for secified analysis as well as choose the analytical method. Student is able to perform specified determinations and analysis.		2,0
3,0The student's knowledge is at the level of 60%
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_B05_K01
Student can make the initial assesment and choose an analytical method/technique required for characterisation of particular material/product. Student is able to work in team to achive particular effect of characterisation of tested materials/products.		2,0
3,0The student's knowledge is at the level of 60%
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. J.A Iggo, K.V.Lyzyanin, NMR spectroscopy in inorganic chemistry, Oxford University Press, Oxford, 2020
  2. Kazuo Nakamoto, Infrared and Raman Spectra of Inorganic and Coordination Compounds, Part A: Theory and Applications in Inorganic Chemistry, John Wiley&Sons, 2008, 6
  3. Pungar Erno, A practical guide to instrumental analysis, CRC Press, 2020
  4. Petrozzi Sergio, Practical instrumental analysis, John Wiley & Sons, 2012
  5. D. Muralidhara Rao, Instrumental Methods of Analysis, CBS Publishers & Distributors Private Limited, 2020
  6. SOMENATH MITRA, Sample Preparation Techniques in Analytical Chemistry, John Wiley & Sons, 2003
  7. Ferenc Paulik, Special trends in thermal analysis, John Wiley & Sons, 1995, 1 or later

Literatura dodatkowa

  1. J. A. Gadsden Aric, Infrared Spectra of Minerals and Related Inorganic Compounds, BUTTERWORTHS, 1975
  2. R. A. Nyquist, R. O. Kagel, Infrared spectra of inorganic compounds, vol. 4, Academic Press Inc., 1997
  3. Robert Dinnebier,.; Andreas Leineweber, ; John S.O. Evans, Rietveld Refinement (de Gruyter Stem) Illustrated Edition, ‎ de Gruyter, 2018, ISBN-13: 978-3110456219 ISBN-10: 3110456214
  4. R. A. Young (Editor), The Rietveld Method (International Union of Crystallography Monographs on Crystallography, 5), Oxford University Press, Oxford, 1995, ISBN-13: 9780198559122

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Characterisation of catalytic materials10
T-L-2Characterisation of carbon materials10
T-L-3Characterisation of fertilizers5
T-L-4XRD as a tool for investigation of amorphous, semicrystaline and crystalline materials5
T-L-5Analysis of IR spectra of various groups of inorganic compounds.5
T-L-6Application of the DTA and TG methods for testing inorganic substances and their mixtures (thermal stability, temperature and way of melting, thermal decomposition mechanism etc.).5
T-L-7Analysis of NMR and CP MAS spectra of inorganic compounds. Case study.5
45

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Methods of sampling and prepatation of samples for analysis2
T-W-2Application of specified methods/techniques for characterisation of inorganic products like catalysts, carbon materials and fertilizers, such as: XRF, XPS, SEM/EDX, BET, DLS, UVvis/DRS, ICP, elemental analysis (O, N, H, C, S)8
T-W-3Solving of the crystal structure2
T-W-4Rietveld refinement2
T-W-5XRD investigations of amorphous, semicrystaline and crystalline materials2
T-W-6Introduction to IR spectroscopy. Overview of instrumentation to use to study of inorganic compound. Applications in inorganic chemistry (merits and demerits).4
T-W-7Thermal analysis methods, their division and scope of applications. Selected measurement techniques: Differential thermal analysis (DTA) and thermogravimetry (TG). Physicochemical phenomena during thermal processing of solids. Recorded effects and their characteristic parameters.2
T-W-8Influence of measurement conditions (sample mass, particle size, gas atmosphere, heating rate, sample container shape) on the test result.2
T-W-9Quantitative and qualitative interpretation of DTA, TG results. Examples of special applications of thermal analysis methods for the determination of substance properties and the construction of phase diagrams.2
T-W-10NMR and CP MAS NMR of nuclei others than 1H and 13C. Equippments, practical applications and limitations.4
30

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1Obligatory attendance at the classes45
A-L-2Preparation of the reports5
50
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Attendance at the lectures30
A-W-2Individual literature studies10
A-W-3Preparation for the exam10
50
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_B05_W01Student knows the methods of inorganic samples collecting and preparation for instrumental analysis. Student understands the basics of the analytical procedures and the criteria for for selection of particular techniques depending on the purpose of the analysis
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_W01Graduate has in-depth knowledge in the field of chemical processes, including appropriate selection of materials, raw materials, methods, techniques, equipment and devices for the implementation of chemical and biochemical processes and characterization of the raw materials and products obtained.
Cel przedmiotuC-1Student knows specified testing/analysis techniques of the basic parameters of inorganic products/materials
Treści programoweT-W-10NMR and CP MAS NMR of nuclei others than 1H and 13C. Equippments, practical applications and limitations.
T-L-7Analysis of NMR and CP MAS spectra of inorganic compounds. Case study.
T-W-3Solving of the crystal structure
T-W-4Rietveld refinement
T-W-5XRD investigations of amorphous, semicrystaline and crystalline materials
T-L-4XRD as a tool for investigation of amorphous, semicrystaline and crystalline materials
T-W-1Methods of sampling and prepatation of samples for analysis
T-W-2Application of specified methods/techniques for characterisation of inorganic products like catalysts, carbon materials and fertilizers, such as: XRF, XPS, SEM/EDX, BET, DLS, UVvis/DRS, ICP, elemental analysis (O, N, H, C, S)
T-L-1Characterisation of catalytic materials
T-L-2Characterisation of carbon materials
T-L-3Characterisation of fertilizers
T-W-6Introduction to IR spectroscopy. Overview of instrumentation to use to study of inorganic compound. Applications in inorganic chemistry (merits and demerits).
T-L-5Analysis of IR spectra of various groups of inorganic compounds.
T-L-6Application of the DTA and TG methods for testing inorganic substances and their mixtures (thermal stability, temperature and way of melting, thermal decomposition mechanism etc.).
T-W-7Thermal analysis methods, their division and scope of applications. Selected measurement techniques: Differential thermal analysis (DTA) and thermogravimetry (TG). Physicochemical phenomena during thermal processing of solids. Recorded effects and their characteristic parameters.
T-W-8Influence of measurement conditions (sample mass, particle size, gas atmosphere, heating rate, sample container shape) on the test result.
T-W-9Quantitative and qualitative interpretation of DTA, TG results. Examples of special applications of thermal analysis methods for the determination of substance properties and the construction of phase diagrams.
Metody nauczaniaM-1Lecture
M-2Laboratory
Sposób ocenyS-1Ocena podsumowująca: Laboratory - attendance and reports
S-2Ocena podsumowująca: Lecture - exam
Kryteria ocenyOcenaKryterium oceny
2,0
3,0The student's knowledge is at the level of 60%
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_B05_U01Student can choose the method of sampling and preparing samples for secified analysis as well as choose the analytical method. Student is able to perform specified determinations and analysis.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_U01Graduate is able to utilize the in-depth knowledge in the field of chemical processes, including appropriate selection of materials, raw materials, methods, techniques, equipment and devices for the implementation of chemical and biochemical processes and characterization of the raw materials and products obtained.
Cel przedmiotuC-1Student knows specified testing/analysis techniques of the basic parameters of inorganic products/materials
Treści programoweT-W-10NMR and CP MAS NMR of nuclei others than 1H and 13C. Equippments, practical applications and limitations.
T-L-7Analysis of NMR and CP MAS spectra of inorganic compounds. Case study.
T-W-3Solving of the crystal structure
T-W-4Rietveld refinement
T-W-5XRD investigations of amorphous, semicrystaline and crystalline materials
T-L-4XRD as a tool for investigation of amorphous, semicrystaline and crystalline materials
T-W-1Methods of sampling and prepatation of samples for analysis
T-W-2Application of specified methods/techniques for characterisation of inorganic products like catalysts, carbon materials and fertilizers, such as: XRF, XPS, SEM/EDX, BET, DLS, UVvis/DRS, ICP, elemental analysis (O, N, H, C, S)
T-L-1Characterisation of catalytic materials
T-L-2Characterisation of carbon materials
T-L-3Characterisation of fertilizers
T-W-6Introduction to IR spectroscopy. Overview of instrumentation to use to study of inorganic compound. Applications in inorganic chemistry (merits and demerits).
T-L-5Analysis of IR spectra of various groups of inorganic compounds.
T-L-6Application of the DTA and TG methods for testing inorganic substances and their mixtures (thermal stability, temperature and way of melting, thermal decomposition mechanism etc.).
T-W-7Thermal analysis methods, their division and scope of applications. Selected measurement techniques: Differential thermal analysis (DTA) and thermogravimetry (TG). Physicochemical phenomena during thermal processing of solids. Recorded effects and their characteristic parameters.
T-W-8Influence of measurement conditions (sample mass, particle size, gas atmosphere, heating rate, sample container shape) on the test result.
T-W-9Quantitative and qualitative interpretation of DTA, TG results. Examples of special applications of thermal analysis methods for the determination of substance properties and the construction of phase diagrams.
Metody nauczaniaM-1Lecture
M-2Laboratory
Sposób ocenyS-1Ocena podsumowująca: Laboratory - attendance and reports
S-2Ocena podsumowująca: Lecture - exam
Kryteria ocenyOcenaKryterium oceny
2,0
3,0The student's knowledge is at the level of 60%
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_B05_K01Student can make the initial assesment and choose an analytical method/technique required for characterisation of particular material/product. Student is able to work in team to achive particular effect of characterisation of tested materials/products.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_K02Graduate is aware of the importance of knowledge in solving of cognitive and practical problems and is ready to consult experts in the case of difficult problems.
Cel przedmiotuC-1Student knows specified testing/analysis techniques of the basic parameters of inorganic products/materials
Treści programoweT-W-10NMR and CP MAS NMR of nuclei others than 1H and 13C. Equippments, practical applications and limitations.
T-L-7Analysis of NMR and CP MAS spectra of inorganic compounds. Case study.
T-W-3Solving of the crystal structure
T-W-4Rietveld refinement
T-W-5XRD investigations of amorphous, semicrystaline and crystalline materials
T-L-4XRD as a tool for investigation of amorphous, semicrystaline and crystalline materials
T-W-1Methods of sampling and prepatation of samples for analysis
T-W-2Application of specified methods/techniques for characterisation of inorganic products like catalysts, carbon materials and fertilizers, such as: XRF, XPS, SEM/EDX, BET, DLS, UVvis/DRS, ICP, elemental analysis (O, N, H, C, S)
T-L-1Characterisation of catalytic materials
T-L-2Characterisation of carbon materials
T-L-3Characterisation of fertilizers
T-W-6Introduction to IR spectroscopy. Overview of instrumentation to use to study of inorganic compound. Applications in inorganic chemistry (merits and demerits).
T-L-5Analysis of IR spectra of various groups of inorganic compounds.
T-L-6Application of the DTA and TG methods for testing inorganic substances and their mixtures (thermal stability, temperature and way of melting, thermal decomposition mechanism etc.).
T-W-7Thermal analysis methods, their division and scope of applications. Selected measurement techniques: Differential thermal analysis (DTA) and thermogravimetry (TG). Physicochemical phenomena during thermal processing of solids. Recorded effects and their characteristic parameters.
T-W-8Influence of measurement conditions (sample mass, particle size, gas atmosphere, heating rate, sample container shape) on the test result.
T-W-9Quantitative and qualitative interpretation of DTA, TG results. Examples of special applications of thermal analysis methods for the determination of substance properties and the construction of phase diagrams.
Metody nauczaniaM-1Lecture
M-2Laboratory
Sposób ocenyS-1Ocena podsumowująca: Laboratory - attendance and reports
S-2Ocena podsumowująca: Lecture - exam
Kryteria ocenyOcenaKryterium oceny
2,0
3,0The student's knowledge is at the level of 60%
3,5
4,0
4,5
5,0