Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Administracja Centralna Uczelni - Wymiana międzynarodowa (S1)

Sylabus przedmiotu CHROMATOGRAPHIC METHODS:

Informacje podstawowe

Kierunek studiów Wymiana międzynarodowa
Forma studiów studia stacjonarne Poziom pierwszego stopnia
Tytuł zawodowy absolwenta
Obszary studiów
Profil
Moduł
Przedmiot CHROMATOGRAPHIC METHODS
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Technologii Chemicznej Organicznej i Materiałów Polimerowych
Nauczyciel odpowiedzialny Małgorzata Dzięcioł <Malgorzata.Dzieciol@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 6,0 ECTS (formy) 6,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny Grupa obieralna

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
wykładyW1 15 1,00,40zaliczenie
laboratoriaL1 30 4,00,40zaliczenie
ćwiczenia audytoryjneA1 15 1,00,20zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Basic knowledge of organic chemistry

Cele przedmiotu

KODCel modułu/przedmiotu
C-1Knowledge of theoretical and practical aspects of chromatographic methods and their applications.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
ćwiczenia audytoryjne
T-A-1Chromatographic data analysis. Mass spectra analysis. Calculations related to peaks resolution, polarity and performance of chromatographic columns, retention parameters, identification and quantification of compounds. Application of chromatographic methods in the analysis of selected groups of analytes. Written assignments from the elaborated topics.15
15
laboratoria
T-L-1Maintenance and method development in gas chromatography. Evaluation of separation efficiency. Qualitative and quantitative analysis in gas chromatography.10
T-L-2Application of GC-MS method in identification and quantification of compounds.10
T-L-3Qualitative and quantitative analysis in liquid chromatography.10
30
wykłady
T-W-1General theory of chromatography. Classification of chromatographic methods. Retention parameters. Resolution. Separation efficiency of column. Identification and quantification methods in chromatography.5
T-W-2Gas chromatography (GC) – principles, instrumentation, carrier gas, columns and stationary phases, sampling, detectors, applications.5
T-W-3High performance liquid chromatography (HPLC) – instrumentation, eluents, stationary phases, normal and reversed-phase chromatography, isocratic and gradient elution, detectors, applications.3
T-W-4Thin layer chromatography (TLC) – principles, adsorbents and plates, chambers, development techniques, densitometry.1
T-W-5Written test (grade)1
15

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
ćwiczenia audytoryjne
A-A-1Participation in auditory classes15
A-A-2Studying of the literature and other recommended materials10
25
laboratoria
A-L-1Theoretical preparation for the laboratory20
A-L-2Participation in laboratory classes30
A-L-3Preparation of written reports50
100
wykłady
A-W-1Participation in lectures15
A-W-2Studying of literature and learning8
A-W-3Consultations2
25

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Lecture with presentation and discussion
M-2Auditory classes
M-3Laboratory
M-4Consultations

Sposoby oceny

KODSposób oceny
S-1Ocena formująca: Evaluation of working in the laboratory
S-2Ocena formująca: Evaluation of working during auditory classes
S-3Ocena podsumowująca: Lecture: final written test - grade
S-4Ocena podsumowująca: Laboratory: written reports
S-5Ocena podsumowująca: Auditory classes: written assignments

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_1-_null_W01
Student will be able to classify chromatographic methods, describe different chromatographic separation processes and instrumentation used in chromatography.
C-1T-L-1, T-W-1, T-W-3, T-W-4M-1, M-4S-3

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_1-_null_U01
Student will be able to apply chromatographic methods in order to perform qualitative and quantitative analysis of organic compounds.
C-1T-L-1, T-L-2, T-L-3M-1, M-3, M-4S-1, S-4
WM-WTiICh_1-_null_U02
Student is able to analyze and elaborate chromatographic data and perform necessary calculations.
C-1T-L-2, T-W-2, T-A-1, T-L-1, T-W-1, T-W-4, T-W-3, T-L-3M-3, M-2, M-4S-5, S-4, S-1, S-2

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_1-_null_K01
Student is aware of the responsibility for the results of analyses.
C-1T-L-2, T-L-3, T-L-1M-3, M-4S-1, S-4

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
WM-WTiICh_1-_null_W01
Student will be able to classify chromatographic methods, describe different chromatographic separation processes and instrumentation used in chromatography.
2,0
3,0student is able to describe the theoretical basics of chromatographic methods
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
WM-WTiICh_1-_null_U01
Student will be able to apply chromatographic methods in order to perform qualitative and quantitative analysis of organic compounds.
2,0
3,0student is able to perform analysis with the help of a teacher
3,5
4,0
4,5
5,0
WM-WTiICh_1-_null_U02
Student is able to analyze and elaborate chromatographic data and perform necessary calculations.
2,0
3,0student is able to analyze and elaborate chromatographic data with the help of a teacher
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
WM-WTiICh_1-_null_K01
Student is aware of the responsibility for the results of analyses.
2,0
3,0student submits for evaluation written reports containing verified results
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. Braithwaite A., Smith F.J., Chromatographic Methods, Springer, 1996
  2. McNair H.M., Miller J.M., Basic Gas Chromatography, Wiley, 2009, II edition
  3. Snyder L.R., Kirkland J.L., Dolan J.W., Introduction to Modern Liquid Chromatography, Wiley, 2010

Treści programowe - ćwiczenia audytoryjne

KODTreść programowaGodziny
T-A-1Chromatographic data analysis. Mass spectra analysis. Calculations related to peaks resolution, polarity and performance of chromatographic columns, retention parameters, identification and quantification of compounds. Application of chromatographic methods in the analysis of selected groups of analytes. Written assignments from the elaborated topics.15
15

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Maintenance and method development in gas chromatography. Evaluation of separation efficiency. Qualitative and quantitative analysis in gas chromatography.10
T-L-2Application of GC-MS method in identification and quantification of compounds.10
T-L-3Qualitative and quantitative analysis in liquid chromatography.10
30

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1General theory of chromatography. Classification of chromatographic methods. Retention parameters. Resolution. Separation efficiency of column. Identification and quantification methods in chromatography.5
T-W-2Gas chromatography (GC) – principles, instrumentation, carrier gas, columns and stationary phases, sampling, detectors, applications.5
T-W-3High performance liquid chromatography (HPLC) – instrumentation, eluents, stationary phases, normal and reversed-phase chromatography, isocratic and gradient elution, detectors, applications.3
T-W-4Thin layer chromatography (TLC) – principles, adsorbents and plates, chambers, development techniques, densitometry.1
T-W-5Written test (grade)1
15

Formy aktywności - ćwiczenia audytoryjne

KODForma aktywnościGodziny
A-A-1Participation in auditory classes15
A-A-2Studying of the literature and other recommended materials10
25
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1Theoretical preparation for the laboratory20
A-L-2Participation in laboratory classes30
A-L-3Preparation of written reports50
100
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Participation in lectures15
A-W-2Studying of literature and learning8
A-W-3Consultations2
25
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_1-_null_W01Student will be able to classify chromatographic methods, describe different chromatographic separation processes and instrumentation used in chromatography.
Cel przedmiotuC-1Knowledge of theoretical and practical aspects of chromatographic methods and their applications.
Treści programoweT-L-1Maintenance and method development in gas chromatography. Evaluation of separation efficiency. Qualitative and quantitative analysis in gas chromatography.
T-W-1General theory of chromatography. Classification of chromatographic methods. Retention parameters. Resolution. Separation efficiency of column. Identification and quantification methods in chromatography.
T-W-3High performance liquid chromatography (HPLC) – instrumentation, eluents, stationary phases, normal and reversed-phase chromatography, isocratic and gradient elution, detectors, applications.
T-W-4Thin layer chromatography (TLC) – principles, adsorbents and plates, chambers, development techniques, densitometry.
Metody nauczaniaM-1Lecture with presentation and discussion
M-4Consultations
Sposób ocenyS-3Ocena podsumowująca: Lecture: final written test - grade
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student is able to describe the theoretical basics of chromatographic methods
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_1-_null_U01Student will be able to apply chromatographic methods in order to perform qualitative and quantitative analysis of organic compounds.
Cel przedmiotuC-1Knowledge of theoretical and practical aspects of chromatographic methods and their applications.
Treści programoweT-L-1Maintenance and method development in gas chromatography. Evaluation of separation efficiency. Qualitative and quantitative analysis in gas chromatography.
T-L-2Application of GC-MS method in identification and quantification of compounds.
T-L-3Qualitative and quantitative analysis in liquid chromatography.
Metody nauczaniaM-1Lecture with presentation and discussion
M-3Laboratory
M-4Consultations
Sposób ocenyS-1Ocena formująca: Evaluation of working in the laboratory
S-4Ocena podsumowująca: Laboratory: written reports
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student is able to perform analysis with the help of a teacher
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_1-_null_U02Student is able to analyze and elaborate chromatographic data and perform necessary calculations.
Cel przedmiotuC-1Knowledge of theoretical and practical aspects of chromatographic methods and their applications.
Treści programoweT-L-2Application of GC-MS method in identification and quantification of compounds.
T-W-2Gas chromatography (GC) – principles, instrumentation, carrier gas, columns and stationary phases, sampling, detectors, applications.
T-A-1Chromatographic data analysis. Mass spectra analysis. Calculations related to peaks resolution, polarity and performance of chromatographic columns, retention parameters, identification and quantification of compounds. Application of chromatographic methods in the analysis of selected groups of analytes. Written assignments from the elaborated topics.
T-L-1Maintenance and method development in gas chromatography. Evaluation of separation efficiency. Qualitative and quantitative analysis in gas chromatography.
T-W-1General theory of chromatography. Classification of chromatographic methods. Retention parameters. Resolution. Separation efficiency of column. Identification and quantification methods in chromatography.
T-W-4Thin layer chromatography (TLC) – principles, adsorbents and plates, chambers, development techniques, densitometry.
T-W-3High performance liquid chromatography (HPLC) – instrumentation, eluents, stationary phases, normal and reversed-phase chromatography, isocratic and gradient elution, detectors, applications.
T-L-3Qualitative and quantitative analysis in liquid chromatography.
Metody nauczaniaM-3Laboratory
M-2Auditory classes
M-4Consultations
Sposób ocenyS-5Ocena podsumowująca: Auditory classes: written assignments
S-4Ocena podsumowująca: Laboratory: written reports
S-1Ocena formująca: Evaluation of working in the laboratory
S-2Ocena formująca: Evaluation of working during auditory classes
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student is able to analyze and elaborate chromatographic data with the help of a teacher
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_1-_null_K01Student is aware of the responsibility for the results of analyses.
Cel przedmiotuC-1Knowledge of theoretical and practical aspects of chromatographic methods and their applications.
Treści programoweT-L-2Application of GC-MS method in identification and quantification of compounds.
T-L-3Qualitative and quantitative analysis in liquid chromatography.
T-L-1Maintenance and method development in gas chromatography. Evaluation of separation efficiency. Qualitative and quantitative analysis in gas chromatography.
Metody nauczaniaM-3Laboratory
M-4Consultations
Sposób ocenyS-1Ocena formująca: Evaluation of working in the laboratory
S-4Ocena podsumowująca: Laboratory: written reports
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student submits for evaluation written reports containing verified results
3,5
4,0
4,5
5,0