Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Administracja Centralna Uczelni - Wymiana międzynarodowa (S2)

Sylabus przedmiotu ISOLATION AND CHARACTERIZATION OF NATURAL PRODUCTS FROM PLANTS:

Informacje podstawowe

Kierunek studiów Wymiana międzynarodowa
Forma studiów studia stacjonarne Poziom drugiego stopnia
Tytuł zawodowy absolwenta
Obszary studiów
Profil
Moduł
Przedmiot ISOLATION AND CHARACTERIZATION OF NATURAL PRODUCTS FROM PLANTS
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Technologii Chemicznej Organicznej i Materiałów Polimerowych
Nauczyciel odpowiedzialny Małgorzata Dzięcioł <Malgorzata.Dzieciol@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 5,0 ECTS (formy) 5,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny Grupa obieralna

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
laboratoriaL1 45 5,01,00zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Basics of analytical chemistry

Cele przedmiotu

KODCel modułu/przedmiotu
C-1Knowledge and practical skills related to isolation methods of natural products from plants.
C-2Knowledge and practical skills related to application of chromatographic and spectrophotometric methods to determination of composition and antioxidant activity of natural products isolated from plants.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
laboratoria
T-L-1Isolation of biologically active compounds from plant materials by different techniques including reflux extraction, ultrasound assisted extraction, Soxhlet extraction.15
T-L-2Isolation of essential oils from plant materials by hydrodistillation method by using Deryng or Clevenger-type apparatus. Determination of the yields of essential oils.10
T-L-3Analysis of essential oils and plant extracts composition by gas chromatography with mass selective detector method (GC-MS). Identification of the particular compounds on the basis of their retention times, retention indices and mass spectra.10
T-L-4Analysis of antioxidant activity of extracts and essential oils by spectrophotometric method with DPPH radical. Determination of phenolic compounds by spectrophotometric method with Folin-Ciocalteu reagent.10
45

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
laboratoria
A-L-1Participation in laboratory classes45
A-L-2Preparation for classes - individual work with literature30
A-L-3Elaboration of experimental results15
A-L-4Preparation of written reports30
A-L-5Consultations5
125

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Laboratory
M-2Consultations
M-3Individual work with the literature

Sposoby oceny

KODSposób oceny
S-1Ocena formująca: Evaluation of working in the laboratory
S-2Ocena podsumowująca: Evaluation of written reports

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_null_W01
Student is able to characterize selected methods of isolation and analysis applied for natural products from plants.
C-1, C-2T-L-1, T-L-2, T-L-4, T-L-3M-1, M-2, M-3S-1, S-2

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_null_U01
Student is able to perform experiments using different methods of isolation of natural products from plants.
C-1T-L-1, T-L-2M-1, M-3S-1, S-2
WM-WTiICh_2-_null_U02
Student is able to analyse the composition of natural products by gas chromatography method and determine their antioxidant activity using spectrophotometric methods.
C-2T-L-4, T-L-3M-1, M-2, M-3S-1, S-2

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_null_K01
The student knows the importance of plants as natural sources of biologically active compounds.
C-2T-L-4, T-L-3M-1, M-2, M-3S-1, S-2

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
WM-WTiICh_2-_null_W01
Student is able to characterize selected methods of isolation and analysis applied for natural products from plants.
2,0
3,0student has basic knowledge related to isolation and analysis of natural products from plants
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
WM-WTiICh_2-_null_U01
Student is able to perform experiments using different methods of isolation of natural products from plants.
2,0
3,0student is able to perform experiments using different methods of isolation with the help of a teacher
3,5
4,0
4,5
5,0
WM-WTiICh_2-_null_U02
Student is able to analyse the composition of natural products by gas chromatography method and determine their antioxidant activity using spectrophotometric methods.
2,0
3,0student is able to perform chromatographic and spectrophotometric analyses with the help of a teacher and present their results in written reports
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
WM-WTiICh_2-_null_K01
The student knows the importance of plants as natural sources of biologically active compounds.
2,0
3,0student is able to indicate the main biologically active compounds in selected plants
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. Xu R., Ye Y., Zhao W. (ed.), Introduction to Natural Products Chemistry, CRC Press, Boca Raton, 2012
  2. Sarker S.D., Latif Z., Gray A.I. (ed.), Natural Products Isolation, Humana Press, Totowa, New Jersey, 2006
  3. McNair H.M., Miller J.M., Basic Gas Chromatography, Wiley, 2009, II edition

Literatura dodatkowa

  1. Goyal M.R., Joy P.P., Suleria H.A.R. (ed.), Plant Secondary Metabolites for Human Health: Extraction of Bioactive Compounds, Apple Academic Press, 2019

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Isolation of biologically active compounds from plant materials by different techniques including reflux extraction, ultrasound assisted extraction, Soxhlet extraction.15
T-L-2Isolation of essential oils from plant materials by hydrodistillation method by using Deryng or Clevenger-type apparatus. Determination of the yields of essential oils.10
T-L-3Analysis of essential oils and plant extracts composition by gas chromatography with mass selective detector method (GC-MS). Identification of the particular compounds on the basis of their retention times, retention indices and mass spectra.10
T-L-4Analysis of antioxidant activity of extracts and essential oils by spectrophotometric method with DPPH radical. Determination of phenolic compounds by spectrophotometric method with Folin-Ciocalteu reagent.10
45

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1Participation in laboratory classes45
A-L-2Preparation for classes - individual work with literature30
A-L-3Elaboration of experimental results15
A-L-4Preparation of written reports30
A-L-5Consultations5
125
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_2-_null_W01Student is able to characterize selected methods of isolation and analysis applied for natural products from plants.
Cel przedmiotuC-1Knowledge and practical skills related to isolation methods of natural products from plants.
C-2Knowledge and practical skills related to application of chromatographic and spectrophotometric methods to determination of composition and antioxidant activity of natural products isolated from plants.
Treści programoweT-L-1Isolation of biologically active compounds from plant materials by different techniques including reflux extraction, ultrasound assisted extraction, Soxhlet extraction.
T-L-2Isolation of essential oils from plant materials by hydrodistillation method by using Deryng or Clevenger-type apparatus. Determination of the yields of essential oils.
T-L-4Analysis of antioxidant activity of extracts and essential oils by spectrophotometric method with DPPH radical. Determination of phenolic compounds by spectrophotometric method with Folin-Ciocalteu reagent.
T-L-3Analysis of essential oils and plant extracts composition by gas chromatography with mass selective detector method (GC-MS). Identification of the particular compounds on the basis of their retention times, retention indices and mass spectra.
Metody nauczaniaM-1Laboratory
M-2Consultations
M-3Individual work with the literature
Sposób ocenyS-1Ocena formująca: Evaluation of working in the laboratory
S-2Ocena podsumowująca: Evaluation of written reports
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student has basic knowledge related to isolation and analysis of natural products from plants
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_2-_null_U01Student is able to perform experiments using different methods of isolation of natural products from plants.
Cel przedmiotuC-1Knowledge and practical skills related to isolation methods of natural products from plants.
Treści programoweT-L-1Isolation of biologically active compounds from plant materials by different techniques including reflux extraction, ultrasound assisted extraction, Soxhlet extraction.
T-L-2Isolation of essential oils from plant materials by hydrodistillation method by using Deryng or Clevenger-type apparatus. Determination of the yields of essential oils.
Metody nauczaniaM-1Laboratory
M-3Individual work with the literature
Sposób ocenyS-1Ocena formująca: Evaluation of working in the laboratory
S-2Ocena podsumowująca: Evaluation of written reports
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student is able to perform experiments using different methods of isolation with the help of a teacher
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_2-_null_U02Student is able to analyse the composition of natural products by gas chromatography method and determine their antioxidant activity using spectrophotometric methods.
Cel przedmiotuC-2Knowledge and practical skills related to application of chromatographic and spectrophotometric methods to determination of composition and antioxidant activity of natural products isolated from plants.
Treści programoweT-L-4Analysis of antioxidant activity of extracts and essential oils by spectrophotometric method with DPPH radical. Determination of phenolic compounds by spectrophotometric method with Folin-Ciocalteu reagent.
T-L-3Analysis of essential oils and plant extracts composition by gas chromatography with mass selective detector method (GC-MS). Identification of the particular compounds on the basis of their retention times, retention indices and mass spectra.
Metody nauczaniaM-1Laboratory
M-2Consultations
M-3Individual work with the literature
Sposób ocenyS-1Ocena formująca: Evaluation of working in the laboratory
S-2Ocena podsumowująca: Evaluation of written reports
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student is able to perform chromatographic and spectrophotometric analyses with the help of a teacher and present their results in written reports
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_2-_null_K01The student knows the importance of plants as natural sources of biologically active compounds.
Cel przedmiotuC-2Knowledge and practical skills related to application of chromatographic and spectrophotometric methods to determination of composition and antioxidant activity of natural products isolated from plants.
Treści programoweT-L-4Analysis of antioxidant activity of extracts and essential oils by spectrophotometric method with DPPH radical. Determination of phenolic compounds by spectrophotometric method with Folin-Ciocalteu reagent.
T-L-3Analysis of essential oils and plant extracts composition by gas chromatography with mass selective detector method (GC-MS). Identification of the particular compounds on the basis of their retention times, retention indices and mass spectra.
Metody nauczaniaM-1Laboratory
M-2Consultations
M-3Individual work with the literature
Sposób ocenyS-1Ocena formująca: Evaluation of working in the laboratory
S-2Ocena podsumowująca: Evaluation of written reports
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student is able to indicate the main biologically active compounds in selected plants
3,5
4,0
4,5
5,0