ZUT - Krajowe Ramy Kwalifikacji / Rok 2018/2019 / Administracja Centralna Uczelni / Wymiana międzynarodowa (S1) / Sylabus przedmiotu

Administracja Centralna Uczelni - Wymiana międzynarodowa (S1)

Sylabus przedmiotu PRINCIPLES OF ANALYTICAL CHEMISTRY:

Informacje podstawowe

Kierunek studiów	Wymiana międzynarodowa
Forma studiów	studia stacjonarne	Poziom	pierwszego stopnia
Tytuł zawodowy absolwenta
Obszary studiów	—
Profil
Moduł	—
Przedmiot	PRINCIPLES OF ANALYTICAL CHEMISTRY
Specjalność	przedmiot wspólny
Jednostka prowadząca	Katedra Chemii Nieorganicznej i Analitycznej
Nauczyciel odpowiedzialny	Zbigniew Rozwadowski <Zbigniew.Rozwadowski@zut.edu.pl>
Inni nauczyciele	Beata Kołodziej <Beata.Kolodziej@zut.edu.pl>, Zbigniew Rozwadowski <Zbigniew.Rozwadowski@zut.edu.pl>
ECTS (planowane)	3,0	ECTS (formy)	3,0
Forma zaliczenia	zaliczenie	Język	polski
Blok obieralny	—	Grupa obieralna	—

Formy dydaktyczne

Forma dydaktyczna	KOD	Semestr	Godziny	ECTS	Waga	Zaliczenie
wykłady	W	2	15	1,0	0,40	zaliczenie
laboratoria	L	2	30	2,0	0,60	zaliczenie

Wymagania wstępne

KOD	Wymaganie wstępne
W-1	The basic knowledge of fundamental and inorganic chemistry as well as basic safety rules

Cele przedmiotu

KOD	Cel modułu/przedmiotu
C-1	Application of an appropriate analytical techniques depending on the sample type and matrix.
C-2	Explanation of the construction of analytical instrumentation and indications the possibility of its application.
C-3	Correct interpretation of the results of analytical determinations. Writing of reports on the analytical results.

Treści programowe z podziałem na formy zajęć

KOD	Treść programowa	Godziny
laboratoria
T-L-1	Occupational health and safety in the laboratory. Calibration of volumetric glassware: calibration of a buret	2
T-L-2	Acid-base titrimetry. Preparation of 0.1 M HCl solution Standardization of 0.1 HCl solution with sodium carbonate.	4
T-L-3	Acid-base titrimetry. Preparation of 0.1 M NaOH solution. Standardization of 0.1 NaOH solution. Titration of HCl solution	5
T-L-4	Conductometry. Conductometric titratiof of HCl	3
T-L-5	Reduction-Oxidation Titrations. Preparation of 0.1 M potassium permanganate solution Standardization of a 0.1 M potassium permanganate solution solution with sodium oxalate. Determination of Fe in sample.	9
T-L-6	Complexometric methods. Determination of total hardness of water	5
T-L-7	Gravimetric methods. Determination of chlorides (Mohr method)	2
		30
wykłady
T-W-1	Basic tool in analytical chemistry (measurements, concentration, stock solution, basic equippment, etc.). Analytical methods (accuracy, selectivity, sensitivity, experimental errors, statistical analysis of data). Standarizing analytical methods. Preparation of samples.	4
T-W-2	Titrametic methods (acid-base, complexation, redox, precipitation). Gravimetric methods.	5
T-W-3	Spectroscopic methods (UV-Vis, IR, NMR, etc.).	3
T-W-4	Chromatographic methods (GC, HPLC).	2
T-W-5	Electrochemical methods: introduction to electrochemistry, conductometry, potentiometry, amperometry and voltametry.	1
		15

Obciążenie pracą studenta - formy aktywności

KOD	Forma aktywności	Godziny
laboratoria
A-L-1	Participation in classes (labs)	30
A-L-2	Preparation for practical classes	10
A-L-3	Development of results	15
A-L-4	Writing of class reports	5
		60
wykłady
A-W-1	Participation in lectures	15
A-W-2	Preparation for exam	15
		30

Metody nauczania / narzędzia dydaktyczne

KOD	Metoda nauczania / narzędzie dydaktyczne
M-1	Lecture
M-2	Discussion
M-3	Labs

Sposoby oceny

KOD	Sposób oceny
S-1	Ocena podsumowująca: Written exam (lecture)
S-2	Ocena podsumowująca: Continuous assessment: lab reports and activity (labs)

Zamierzone efekty kształcenia - wiedza

Zamierzone efekty kształcenia	Odniesienie do efektów kształcenia dla kierunku studiów	Odniesienie do efektów zdefiniowanych dla obszaru kształcenia	Cel przedmiotu	Treści programowe	Metody nauczania	Sposób oceny
WM-WTiICh_1-_??_W01 Knowledge of the analytical techniques and analytical procedures	—	—	C-1, C-3, C-2	T-W-1, T-W-5, T-W-2, T-W-4, T-W-3	M-1, M-2	S-1

Zamierzone efekty kształcenia - umiejętności

Zamierzone efekty kształcenia	Odniesienie do efektów kształcenia dla kierunku studiów	Odniesienie do efektów zdefiniowanych dla obszaru kształcenia	Cel przedmiotu	Treści programowe	Metody nauczania	Sposób oceny
WM-WTiICh_1-_??_U01 Explanation of the construction of analytical instrumentation and indications the possibility of its application.	—	—	C-1, C-2	T-L-5, T-L-2, T-L-4, T-L-7, T-L-6, T-L-3	M-3, M-1, M-2	S-2

Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne

Zamierzone efekty kształcenia	Odniesienie do efektów kształcenia dla kierunku studiów	Odniesienie do efektów zdefiniowanych dla obszaru kształcenia	Cel przedmiotu	Treści programowe	Metody nauczania	Sposób oceny
WM-WTiICh_1-_??_K01 Correct interpretation of the results	—	—	C-3	T-L-1, T-L-2, T-L-7, T-L-4, T-L-3, T-L-5, T-L-6	M-2, M-3	S-2

Kryterium oceny - wiedza

Efekt kształcenia	Ocena	Kryterium oceny
WM-WTiICh_1-_??_W01 Knowledge of the analytical techniques and analytical procedures	2,0
	3,0	Min. 60% of scoring
	3,5
	4,0
	4,5
	5,0

Kryterium oceny - umiejętności

Efekt kształcenia	Ocena	Kryterium oceny
WM-WTiICh_1-_??_U01 Explanation of the construction of analytical instrumentation and indications the possibility of its application.	2,0
	3,0	Positive grades of lab reports
	3,5
	4,0
	4,5
	5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt kształcenia	Ocena	Kryterium oceny
WM-WTiICh_1-_??_K01 Correct interpretation of the results	2,0
	3,0	Positive grades of lab reports
	3,5
	4,0
	4,5
	5,0

Literatura podstawowa

Harvey D., Modern analytical chemistry, McGraw-Hill Companies Inc., 2000, open access
Curreli, G., Analytical instrumentation, Wiley, Chichester, 2000

Treści programowe - laboratoria

KOD	Treść programowa	Godziny
T-L-1	Occupational health and safety in the laboratory. Calibration of volumetric glassware: calibration of a buret	2
T-L-2	Acid-base titrimetry. Preparation of 0.1 M HCl solution Standardization of 0.1 HCl solution with sodium carbonate.	4
T-L-3	Acid-base titrimetry. Preparation of 0.1 M NaOH solution. Standardization of 0.1 NaOH solution. Titration of HCl solution	5
T-L-4	Conductometry. Conductometric titratiof of HCl	3
T-L-5	Reduction-Oxidation Titrations. Preparation of 0.1 M potassium permanganate solution Standardization of a 0.1 M potassium permanganate solution solution with sodium oxalate. Determination of Fe in sample.	9
T-L-6	Complexometric methods. Determination of total hardness of water	5
T-L-7	Gravimetric methods. Determination of chlorides (Mohr method)	2
		30

Treści programowe - wykłady

KOD	Treść programowa	Godziny
T-W-1	Basic tool in analytical chemistry (measurements, concentration, stock solution, basic equippment, etc.). Analytical methods (accuracy, selectivity, sensitivity, experimental errors, statistical analysis of data). Standarizing analytical methods. Preparation of samples.	4
T-W-2	Titrametic methods (acid-base, complexation, redox, precipitation). Gravimetric methods.	5
T-W-3	Spectroscopic methods (UV-Vis, IR, NMR, etc.).	3
T-W-4	Chromatographic methods (GC, HPLC).	2
T-W-5	Electrochemical methods: introduction to electrochemistry, conductometry, potentiometry, amperometry and voltametry.	1
		15

Formy aktywności - laboratoria

KOD	Forma aktywności	Godziny
A-L-1	Participation in classes (labs)	30
A-L-2	Preparation for practical classes	10
A-L-3	Development of results	15
A-L-4	Writing of class reports	5
		60

(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KOD	Forma aktywności	Godziny
A-W-1	Participation in lectures	15
A-W-2	Preparation for exam	15
		30

(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Pole	KOD	Znaczenie kodu
Zamierzone efekty kształcenia	WM-WTiICh_1-_??_W01	Knowledge of the analytical techniques and analytical procedures
Cel przedmiotu	C-1	Application of an appropriate analytical techniques depending on the sample type and matrix.
	C-3	Correct interpretation of the results of analytical determinations. Writing of reports on the analytical results.
	C-2	Explanation of the construction of analytical instrumentation and indications the possibility of its application.
Treści programowe	T-W-1	Basic tool in analytical chemistry (measurements, concentration, stock solution, basic equippment, etc.). Analytical methods (accuracy, selectivity, sensitivity, experimental errors, statistical analysis of data). Standarizing analytical methods. Preparation of samples.
	T-W-5	Electrochemical methods: introduction to electrochemistry, conductometry, potentiometry, amperometry and voltametry.
	T-W-2	Titrametic methods (acid-base, complexation, redox, precipitation). Gravimetric methods.
	T-W-4	Chromatographic methods (GC, HPLC).
	T-W-3	Spectroscopic methods (UV-Vis, IR, NMR, etc.).
Metody nauczania	M-1	Lecture
Metody nauczania	M-2	Discussion
Sposób oceny	S-1	Ocena podsumowująca: Written exam (lecture)
Kryteria oceny	Ocena	Kryterium oceny
	2,0
	3,0	Min. 60% of scoring
	3,5
	4,0
	4,5
	5,0

Pole	KOD	Znaczenie kodu
Zamierzone efekty kształcenia	WM-WTiICh_1-_??_U01	Explanation of the construction of analytical instrumentation and indications the possibility of its application.
Cel przedmiotu	C-1	Application of an appropriate analytical techniques depending on the sample type and matrix.
Cel przedmiotu	C-2	Explanation of the construction of analytical instrumentation and indications the possibility of its application.
Treści programowe	T-L-5	Reduction-Oxidation Titrations. Preparation of 0.1 M potassium permanganate solution Standardization of a 0.1 M potassium permanganate solution solution with sodium oxalate. Determination of Fe in sample.
	T-L-2	Acid-base titrimetry. Preparation of 0.1 M HCl solution Standardization of 0.1 HCl solution with sodium carbonate.
	T-L-4	Conductometry. Conductometric titratiof of HCl
	T-L-7	Gravimetric methods. Determination of chlorides (Mohr method)
	T-L-6	Complexometric methods. Determination of total hardness of water
	T-L-3	Acid-base titrimetry. Preparation of 0.1 M NaOH solution. Standardization of 0.1 NaOH solution. Titration of HCl solution
Metody nauczania	M-3	Labs
	M-1	Lecture
	M-2	Discussion
Sposób oceny	S-2	Ocena podsumowująca: Continuous assessment: lab reports and activity (labs)
Kryteria oceny	Ocena	Kryterium oceny
	2,0
	3,0	Positive grades of lab reports
	3,5
	4,0
	4,5
	5,0

Pole	KOD	Znaczenie kodu
Zamierzone efekty kształcenia	WM-WTiICh_1-_??_K01	Correct interpretation of the results
Cel przedmiotu	C-3	Correct interpretation of the results of analytical determinations. Writing of reports on the analytical results.
Treści programowe	T-L-1	Occupational health and safety in the laboratory. Calibration of volumetric glassware: calibration of a buret
	T-L-2	Acid-base titrimetry. Preparation of 0.1 M HCl solution Standardization of 0.1 HCl solution with sodium carbonate.
	T-L-7	Gravimetric methods. Determination of chlorides (Mohr method)
	T-L-4	Conductometry. Conductometric titratiof of HCl
	T-L-3	Acid-base titrimetry. Preparation of 0.1 M NaOH solution. Standardization of 0.1 NaOH solution. Titration of HCl solution
	T-L-5	Reduction-Oxidation Titrations. Preparation of 0.1 M potassium permanganate solution Standardization of a 0.1 M potassium permanganate solution solution with sodium oxalate. Determination of Fe in sample.
	T-L-6	Complexometric methods. Determination of total hardness of water
Metody nauczania	M-2	Discussion
Metody nauczania	M-3	Labs
Sposób oceny	S-2	Ocena podsumowująca: Continuous assessment: lab reports and activity (labs)
Kryteria oceny	Ocena	Kryterium oceny
	2,0
	3,0	Positive grades of lab reports
	3,5
	4,0
	4,5
	5,0