Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Wydział Technologii i Inżynierii Chemicznej - Materials Science and Engineering (S1)

Sylabus przedmiotu Structure of Solids:

Informacje podstawowe

Kierunek studiów Materials Science and Engineering
Forma studiów studia stacjonarne Poziom pierwszego stopnia
Tytuł zawodowy absolwenta inżynier
Obszary studiów charakterystyki PRK, kompetencje inżynierskie PRK
Profil ogólnoakademicki
Moduł —
Przedmiot Structure of Solids
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Chemii Nieorganicznej i Analitycznej
Nauczyciel odpowiedzialny Piotr Tabero <Piotr.Tabero@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 5,0 ECTS (formy) 5,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny — Grupa obieralna —

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
wykładyW3 15 1,00,25zaliczenie
laboratoriaL3 45 4,00,75zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Fundamentals of mathematics, physics and chemistry

Cele przedmiotu

KODCel modułu/przedmiotu
C-1Consolidation of basic concepts concerning the structure of solids.
C-2Familiarize students with methods of generation and properties of X-rays.
C-3Expanding knowledge about the measuring techniques using diffraction phenomenon and their practical applications.
C-4Teaching students how to use stuctural data gained from diffraction measurements, available structural databases and literature.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
laboratoria
T-L-1Identification of chemical compounds, metals, alloys and their mixtures.5
T-L-2XRD quantitative phase analysis of various mixtures.5
T-L-3Construction of phase diagrams from XRD data.5
T-L-4X-ray high-temperature measurements. Determination of coefficients of thermal expansion. Anisotropy of thermal expansion. Investigations of polymorphic phase transitions.5
T-L-5Structure solution from owder pattern. Rietveld refinement.5
T-L-6Application of XRD method to verify Hume-Rothery rule and Vegard's law for solid solutions.5
T-L-7Indexation of powder dfiffraction patterns. Lattice parameter determination. Measurement of density. Rentgenographic density.5
T-L-8Determination of grain size, internal stress and lattice distortions.5
T-L-9Aplication of the SAXS method.5
45
wykłady
T-W-1Basic definitions in crystallography. Physical properties of solids. Structure of "ideal" solid.3
T-W-2Crystal systems and Bravais lattices. Symmetry in crystals. Point groups and space groups. International Tables for Crystallography.3
T-W-3Coordination polyhedra. Simple structures of elements and compounds: SC, BCC, FCC and HCP lattices. Types of phase diagrams.2
T-W-4Defects in crystal structure. Solid solutions.2
T-W-5Generation and properties of X-rays. Interaction of X-rays with matter. X-rays diffraction on solids.2
T-W-6Bragg's Law. Investigation of size of crystalites. Indexing of powder diffraction patterns. Determination of the unit cell parameters.3
15

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
laboratoria
A-L-1Participation in laboratories.45
A-L-2Self-study of literature45
A-L-3Preparing for laboratory exercises20
A-L-4Consultations10
120
wykłady
A-W-1Participation in lectures15
A-W-2Consultations2
A-W-3Self-study of the literature12
A-W-4Final written test2
31

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Informative lectures with multimedia instruments, explanation
M-2Work with computers and dedicated software

Sposoby oceny

KODSposób oceny
S-1Ocena podsumowująca: Final written test.
S-2Ocena podsumowująca: written reports

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
MSE_1A_C02_W01
Student knows fundamental concepts in crystallography and knows measuring techniques using diffraction phenomenon		MSE_1A_W02, MSE_1A_W03——C-1, C-2, C-3T-W-1, T-W-2, T-W-3, T-W-4, T-W-5, T-W-6M-1S-1

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
MSE_1A_C02_U01
Students is able to select appropriate diffraction measuring technique to investigate given property of material and interpret obtained results of investigation		MSE_1A_U03——C-1, C-2, C-3T-L-1, T-L-2, T-L-3, T-L-4, T-L-5, T-L-6, T-L-7, T-L-8, T-L-9M-1S-1

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
MSE_1A_C02_K01
Student knows safety procedures for x-ray equipment and understands importance of permanent learning to improve personal competencies		MSE_1A_K04——C-1, C-2, C-3T-L-1, T-L-2, T-L-3, T-L-4, T-L-5, T-L-6, T-L-7, T-L-8, T-L-9M-1S-1

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
MSE_1A_C02_W01
Student knows fundamental concepts in crystallography and knows measuring techniques using diffraction phenomenon		2,0
3,0Student will be able to present basic concepts of crystallography and describe basic measuring methods applying X-ray diffraction.
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
MSE_1A_C02_U01
Students is able to select appropriate diffraction measuring technique to investigate given property of material and interpret obtained results of investigation		2,0
3,0Student will be able to select approprate XRD measuring technique to solve simple problem concerning analysis of crystalline solid
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
MSE_1A_C02_K01
Student knows safety procedures for x-ray equipment and understands importance of permanent learning to improve personal competencies		2,0
3,0Student knows and understands safety procedures for x-ray equipment
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. C. Giacovazzo, H. Z. Monaco, D. Biterbo, F. Scordari, G. Gilli, G. Zanotti, M. Catti, Fundamentals of Crystallography, IUCR, Oxford University Press, Oxford, 2000
  2. D. B. Williams, C. B. Carter, Transmission Electron Microscopy, Plenum Press, New York and London, 1996
  3. O. Engler, V. Randle, Introduction to Texture Analysis. Macrotexture, Microtexture and Orientation Mapping, CRC Press, Taylor & Francis Group, London, New York, 2010
  4. Cullity B.D., Elements of X-ray Diffraction, Addison-Wesley Publishing Company, Inc., London, 1978
  5. P. Luger, Modern X-ray Analysis on Single Crystals, Walter de Gruyter and Co., Berlin, 1980
  6. Glusker, J. P.; Lewis, M.; Rossi, M., “Crystal Structure Analysis for Chemists and Biologists, VCH, New York, 1994
  7. W.I.F. David, K. Shankland, L.B. McCusker and Ch. Baerlocher, Edt., Structure determination form powder diffraction data. IUCr Monographs on crystallography, Oxford Science Publications, Oxford, 2002
  8. A. Gaunier, X-ray Diffraction in Crystals, Imperfect Crystals, and Amorphous Bodies, Courier Corporation, New York, 1994
  9. A. AUTHIER, G. CHAPUIS, EDS, A LITTLE DICTIONARY OF CRYSTALLOGRAPHY, INTERNATIONAL UNION OF CRYSTALLOGRAPHY, 2017, 2ND EDITION
  10. P. P. Ewald, Ed., Fifty Years of X-ray Diffraction, Reprinted in pdf format for the IUCr XVIII Congress, Glasgow, Scotland, Copyright © 1962, 1999 International Union of Crystallography, https://www.iucr.org

Literatura dodatkowa

  1. International Union of Crystallography: https://www.iucr.org
  2. http://www.xtal.iqfr.csic.es/Cristalografia/parte_01_1-en.html

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Identification of chemical compounds, metals, alloys and their mixtures.5
T-L-2XRD quantitative phase analysis of various mixtures.5
T-L-3Construction of phase diagrams from XRD data.5
T-L-4X-ray high-temperature measurements. Determination of coefficients of thermal expansion. Anisotropy of thermal expansion. Investigations of polymorphic phase transitions.5
T-L-5Structure solution from owder pattern. Rietveld refinement.5
T-L-6Application of XRD method to verify Hume-Rothery rule and Vegard's law for solid solutions.5
T-L-7Indexation of powder dfiffraction patterns. Lattice parameter determination. Measurement of density. Rentgenographic density.5
T-L-8Determination of grain size, internal stress and lattice distortions.5
T-L-9Aplication of the SAXS method.5
45

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Basic definitions in crystallography. Physical properties of solids. Structure of "ideal" solid.3
T-W-2Crystal systems and Bravais lattices. Symmetry in crystals. Point groups and space groups. International Tables for Crystallography.3
T-W-3Coordination polyhedra. Simple structures of elements and compounds: SC, BCC, FCC and HCP lattices. Types of phase diagrams.2
T-W-4Defects in crystal structure. Solid solutions.2
T-W-5Generation and properties of X-rays. Interaction of X-rays with matter. X-rays diffraction on solids.2
T-W-6Bragg's Law. Investigation of size of crystalites. Indexing of powder diffraction patterns. Determination of the unit cell parameters.3
15

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1Participation in laboratories.45
A-L-2Self-study of literature45
A-L-3Preparing for laboratory exercises20
A-L-4Consultations10
120
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Participation in lectures15
A-W-2Consultations2
A-W-3Self-study of the literature12
A-W-4Final written test2
31
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięMSE_1A_C02_W01Student knows fundamental concepts in crystallography and knows measuring techniques using diffraction phenomenon
Odniesienie do efektów kształcenia dla kierunku studiówMSE_1A_W02knows selected issues from physics, basic biology and chemistry necessary to describe the properties of materials and processes accompanying their production and processing
MSE_1A_W03knows selected issues concerning the structure of materials, thier synthesis, processing and structure-properties relationship
Cel przedmiotuC-1Consolidation of basic concepts concerning the structure of solids.
C-2Familiarize students with methods of generation and properties of X-rays.
C-3Expanding knowledge about the measuring techniques using diffraction phenomenon and their practical applications.
Treści programoweT-W-1Basic definitions in crystallography. Physical properties of solids. Structure of "ideal" solid.
T-W-2Crystal systems and Bravais lattices. Symmetry in crystals. Point groups and space groups. International Tables for Crystallography.
T-W-3Coordination polyhedra. Simple structures of elements and compounds: SC, BCC, FCC and HCP lattices. Types of phase diagrams.
T-W-4Defects in crystal structure. Solid solutions.
T-W-5Generation and properties of X-rays. Interaction of X-rays with matter. X-rays diffraction on solids.
T-W-6Bragg's Law. Investigation of size of crystalites. Indexing of powder diffraction patterns. Determination of the unit cell parameters.
Metody nauczaniaM-1Informative lectures with multimedia instruments, explanation
Sposób ocenyS-1Ocena podsumowująca: Final written test.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student will be able to present basic concepts of crystallography and describe basic measuring methods applying X-ray diffraction.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięMSE_1A_C02_U01Students is able to select appropriate diffraction measuring technique to investigate given property of material and interpret obtained results of investigation
Odniesienie do efektów kształcenia dla kierunku studiówMSE_1A_U03being able to use the principles and methods of chemistry, biology, physics and materials engineering in planning and conducting experiments, is able to interpret and elaborate the results and draw conclusions
Cel przedmiotuC-1Consolidation of basic concepts concerning the structure of solids.
C-2Familiarize students with methods of generation and properties of X-rays.
C-3Expanding knowledge about the measuring techniques using diffraction phenomenon and their practical applications.
Treści programoweT-L-1Identification of chemical compounds, metals, alloys and their mixtures.
T-L-2XRD quantitative phase analysis of various mixtures.
T-L-3Construction of phase diagrams from XRD data.
T-L-4X-ray high-temperature measurements. Determination of coefficients of thermal expansion. Anisotropy of thermal expansion. Investigations of polymorphic phase transitions.
T-L-5Structure solution from owder pattern. Rietveld refinement.
T-L-6Application of XRD method to verify Hume-Rothery rule and Vegard's law for solid solutions.
T-L-7Indexation of powder dfiffraction patterns. Lattice parameter determination. Measurement of density. Rentgenographic density.
T-L-8Determination of grain size, internal stress and lattice distortions.
T-L-9Aplication of the SAXS method.
Metody nauczaniaM-1Informative lectures with multimedia instruments, explanation
Sposób ocenyS-1Ocena podsumowująca: Final written test.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student will be able to select approprate XRD measuring technique to solve simple problem concerning analysis of crystalline solid
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięMSE_1A_C02_K01Student knows safety procedures for x-ray equipment and understands importance of permanent learning to improve personal competencies
Odniesienie do efektów kształcenia dla kierunku studiówMSE_1A_K04is ready to perform professional roles responsibility, including adherence to the rules of professional ethics and requiring this from others, and care for the achievements and traditions of the profession
Cel przedmiotuC-1Consolidation of basic concepts concerning the structure of solids.
C-2Familiarize students with methods of generation and properties of X-rays.
C-3Expanding knowledge about the measuring techniques using diffraction phenomenon and their practical applications.
Treści programoweT-L-1Identification of chemical compounds, metals, alloys and their mixtures.
T-L-2XRD quantitative phase analysis of various mixtures.
T-L-3Construction of phase diagrams from XRD data.
T-L-4X-ray high-temperature measurements. Determination of coefficients of thermal expansion. Anisotropy of thermal expansion. Investigations of polymorphic phase transitions.
T-L-5Structure solution from owder pattern. Rietveld refinement.
T-L-6Application of XRD method to verify Hume-Rothery rule and Vegard's law for solid solutions.
T-L-7Indexation of powder dfiffraction patterns. Lattice parameter determination. Measurement of density. Rentgenographic density.
T-L-8Determination of grain size, internal stress and lattice distortions.
T-L-9Aplication of the SAXS method.
Metody nauczaniaM-1Informative lectures with multimedia instruments, explanation
Sposób ocenyS-1Ocena podsumowująca: Final written test.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student knows and understands safety procedures for x-ray equipment
3,5
4,0
4,5
5,0