Wydział Technologii i Inżynierii Chemicznej - Chemia (S1)
Sylabus przedmiotu Instrumental Analysis:
Informacje podstawowe
| Kierunek studiów | Chemia | ||
|---|---|---|---|
| Forma studiów | studia stacjonarne | Poziom | pierwszego stopnia |
| Tytuł zawodowy absolwenta | inżynier | ||
| Obszary studiów | charakterystyki PRK, kompetencje inżynierskie PRK | ||
| Profil | ogólnoakademicki | ||
| Moduł | — | ||
| Przedmiot | Instrumental Analysis | ||
| Specjalność | przedmiot wspólny | ||
| Jednostka prowadząca | Katedra Chemii Organicznej i Chemii Fizycznej | ||
| Nauczyciel odpowiedzialny | Elwira Wróblewska <Elwira.Wroblewska@zut.edu.pl> | ||
| Inni nauczyciele | |||
| ECTS (planowane) | 3,0 | ECTS (formy) | 3,0 |
| Forma zaliczenia | zaliczenie | Język | polski |
| Blok obieralny | 3 | Grupa obieralna | 2 |
Formy dydaktyczne
Wymagania wstępne
| KOD | Wymaganie wstępne |
|---|---|
| W-1 | Basis of physical chemistry, organic chemistry, general chemistry, analytical methods. |
Cele przedmiotu
| KOD | Cel modułu/przedmiotu |
|---|---|
| C-1 | Theoretical and practical learning about instrumental methods applied in quantitative and qualitative analysis |
| C-2 | Theoretical studies about the phenomena used in the particular method as well as practical interpretation of the results given. |
Treści programowe z podziałem na formy zajęć
| KOD | Treść programowa | Godziny |
|---|---|---|
| laboratoria | ||
| T-L-1 | Measurements of UV-vis spectra and their application in the studies of solute-solvent intermolecular interaction , as well as in quantitative analysis. | 10 |
| T-L-2 | The interpretation of HNMR spectra as a key to the determination of the structure of organic compounds. | 10 |
| T-L-3 | The application of IR method in qualitative and quantitative analysis of organic compounds. | 10 |
| T-L-4 | The application of chromatographic method in qualitative and quantitative analysis of multicomponent mixtures. | 10 |
| T-L-5 | The determination of some metals with the use of ASA method. | 5 |
| 45 | ||
| wykłady | ||
| T-W-1 | The fundamental definitions concerning analytical process, the kind of analytical method with respect to instrumental method analysis. | 1 |
| T-W-2 | Classification of the methods of instrumental analysis, particularly spectroscopic and chromatographic ones. | 1 |
| T-W-3 | Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties. | 1 |
| T-W-4 | Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation and their application in particular methods i.e. ultraviolet-visual spectroscopy (UV-VIS), infrared spectroscopy (IR), nuclear magnetic resonance spectroscopy (NMR), mass spectroscopy (MS), atomic absorption spectroscopy (AAS), X-ray absorption, atomic emission spectroscopy (AES), flame photometry, inductively coupled plasma spectrometry (ICP), X-ray fluorescence (XRF), atomic fluorescence. | 9 |
| T-W-5 | Explanation of phenomena, concepts, and definitions used in chromatographic methods. The ways of separation of a mixture components. | 3 |
| 15 | ||
Obciążenie pracą studenta - formy aktywności
| KOD | Forma aktywności | Godziny |
|---|---|---|
| laboratoria | ||
| A-L-1 | The participation in the laboratory; the preparation of laboratory report. | 45 |
| A-L-2 | The individual preparation of student for the laboratory. | 5 |
| 50 | ||
| wykłady | ||
| A-W-1 | The participation in the lectures with the possibility of the discussion. | 15 |
| A-W-2 | Individual studies of the subject - reading of the recomended literature. | 5 |
| A-W-3 | The individual preparation of student for the exam. | 5 |
| 25 | ||
Metody nauczania / narzędzia dydaktyczne
| KOD | Metoda nauczania / narzędzie dydaktyczne |
|---|---|
| M-1 | The lectures with the discussion. |
| M-2 | Laboratory |
Sposoby oceny
| KOD | Sposób oceny |
|---|---|
| S-1 | Ocena podsumowująca: Written exam and/or oral discussion. |
| S-2 | Ocena formująca: Assessment of laboratory written report. |
| S-3 | Ocena formująca: Evaluation of the student’s work based on the student activity during the course. |
Zamierzone efekty uczenia się - wiedza
| Zamierzone efekty uczenia się | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Odniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżyniera | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|---|
| KCh_1A_C11b_W01 Student knows the phenomena applied in the instrumental analysis. | KCh_1A_W03 | — | — | C-2 | T-L-1, T-L-2, T-L-3, T-L-4, T-L-5 | M-2 | S-2 |
| KCh_1A_C11b_W02 He has a knowledge about the fundamentals of the selected spectroscopic and chromatographic methods | KCh_1A_W03, KCh_1A_W04 | — | — | C-1, C-2 | T-W-1, T-W-3, T-W-5, T-W-2, T-W-4 | M-1, M-2 | S-1, S-2 |
Zamierzone efekty uczenia się - umiejętności
| Zamierzone efekty uczenia się | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Odniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżyniera | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|---|
| KCh_1A_C11b_U01 Student is able to plan and carry out the experiment with the interpretation of obtained results. | KCh_1A_U04 | — | — | C-1, C-2 | T-L-3, T-L-4, T-L-5, T-L-1, T-L-2 | M-1, M-2 | S-1, S-2 |
Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne
| Zamierzone efekty uczenia się | Odniesienie do efektów kształcenia dla kierunku studiów | Odniesienie do efektów zdefiniowanych dla obszaru kształcenia | Odniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżyniera | Cel przedmiotu | Treści programowe | Metody nauczania | Sposób oceny |
|---|---|---|---|---|---|---|---|
| KCh_1A_C11b_K01 Laboratory exercises conducted in a group allow you to gain ability to cooperate and work in a team. | KCh_1A_K03 | — | — | C-1 | T-L-2, T-L-3, T-L-4, T-L-1, T-L-5 | M-2 | S-2 |
Kryterium oceny - wiedza
| Efekt uczenia się | Ocena | Kryterium oceny |
|---|---|---|
| KCh_1A_C11b_W01 Student knows the phenomena applied in the instrumental analysis. | 2,0 | The student does not have basic knowledge of instrumental analysis and obtained less than 55% of the points in the written examination. |
| 3,0 | The student has basic knowledge in the field of instrumental analysis and obtained between 55% and 64% of points in the written examination. | |
| 3,5 | The student has sufficient knowledge in the field of instrumental analysis and obtained between 64% and 71% of points in the written examination. | |
| 4,0 | The student has good level knowledge in the field of instrumental analysis and obtained between 71% and 80% of points in the written examination. | |
| 4,5 | The student has above-good knowledge in the field of instrumental analysis and obtained between 80% and 89% of points in the written examination. | |
| 5,0 | The student has very good knowledge in the field of instrumental analysis and obtained between 89% and 100% of points in the written examination. | |
| KCh_1A_C11b_W02 He has a knowledge about the fundamentals of the selected spectroscopic and chromatographic methods | 2,0 | The student does not have basic knowledge of instrumental analysis and obtained less than 55% of the points in the written examination. |
| 3,0 | The student has basic knowledge in the field of instrumental analysis and obtained between 55% and 64% of points in the written examination. | |
| 3,5 | The student has sufficient knowledge in the field of instrumental analysis and obtained between 64% and 71% of points in the written examination. | |
| 4,0 | The student has good level knowledge in the field of instrumental analysis and obtained between 71% and 80% of points in the written examination. | |
| 4,5 | The student has above-good knowledge in the field of instrumental analysis and obtained between 80% and 89% of points in the written examination. | |
| 5,0 | The student has very good knowledge in the field of instrumental analysis and obtained between 89% and 100% of points in the written examination. |
Kryterium oceny - umiejętności
| Efekt uczenia się | Ocena | Kryterium oceny |
|---|---|---|
| KCh_1A_C11b_U01 Student is able to plan and carry out the experiment with the interpretation of obtained results. | 2,0 | The student did not acquire the ability to choose an appropriate instrumental method and apply it in the identification/analysis of chemical substances. |
| 3,0 | The student acquired basic skills in selecting an appropriate instrumental method and using it in the identification/analysis of chemical substances. | |
| 3,5 | The student has acquired sufficient skills in selecting an appropriate instrumental method and using it in the identification/analysis of chemical substances. | |
| 4,0 | The student has acquired good skills in selecting an appropriate instrumental method and using it in the identification/analysis of chemical substances. | |
| 4,5 | The student has acquired above-good skills in selecting the appropriate instrumental method and applying it in the identification/analysis of chemical substances. | |
| 5,0 | The student has acquired very good skills in selecting the appropriate instrumental method and using it in the identification/analysis of chemical substances |
Kryterium oceny - inne kompetencje społeczne i personalne
| Efekt uczenia się | Ocena | Kryterium oceny |
|---|---|---|
| KCh_1A_C11b_K01 Laboratory exercises conducted in a group allow you to gain ability to cooperate and work in a team. | 2,0 | The student is unable to cooperate and work in a group. |
| 3,0 | The student is unable to cooperate and work in a group. | |
| 3,5 | The student is unable to cooperate and work in a group. | |
| 4,0 | The student is unable to cooperate and work in a group. | |
| 4,5 | The student is unable to cooperate and work in a group. | |
| 5,0 | The student is unable to cooperate and work in a group. |
Literatura podstawowa
- J. M. Hollas, Modern spectroscopy, John Wiley, 2004
- S. Sternhall, J.R. Kalman, Organic structures from spectra, 3rd ed., Chichester, John Wiley and Son, 2002
- J.R. Chapman, Practical Organic Mass Spectrometry, 2nd ed., Chichester, John Wiley and Son
Literatura dodatkowa
- Ch. Reichardt, Solvents and solvent effects in organic chemistry, 2nd rev. and enl. ed, Weinheim, VCH
- Yoshito Takeuchi and Alan P. Marchand, Applications of NMR spectroscopy to problems in stereochemistry and conformational analysis, Verlag Chemie International, Deerfield Beach, Florida