Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Wydział Technologii i Inżynierii Chemicznej - Chemical Engineering (S2)

Sylabus przedmiotu Modern Organic Synthesis:

Informacje podstawowe

Kierunek studiów Chemical Engineering
Forma studiów studia stacjonarne Poziom drugiego stopnia
Tytuł zawodowy absolwenta magister inżynier
Obszary studiów charakterystyki PRK, kompetencje inżynierskie PRK
Profil ogólnoakademicki
Moduł —
Przedmiot Modern Organic Synthesis
Specjalność Modern and Green Chemical Engineering
Jednostka prowadząca Katedra Chemii Organicznej i Chemii Fizycznej
Nauczyciel odpowiedzialny Jacek Sośnicki <Jacek.Sosnicki@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 3,0 ECTS (formy) 3,0
Forma zaliczenia egzamin Język angielski
Blok obieralny — Grupa obieralna —

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
laboratoriaL2 30 2,00,60zaliczenie
wykładyW2 15 1,00,40egzamin

Wymagania wstępne

KODWymaganie wstępne
W-1Basic knowledge of organic chemistry.

Cele przedmiotu

KODCel modułu/przedmiotu
C-1The student knows how to carry out a basic literature search based on databases and scientific literature.
C-2The student knows the basic methods for construction of a carbon skeleton of organic compounds and knows the various techniques of their synthesis.
C-3The student demonstrates the ability to conduct the basic modern organic chemistry experiments and to analyze data and results by standard analytical methods on a basic level.
C-4The student is aware of the importance of the knowledge acquired within the subject for developement of science and for impovement of the quality of life.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
laboratoria
T-L-1Regulations and safety rules in the laboratory of organic chemistry. Basic and advanced laboratory equipment. Principles of laboratory raport preparation. Introduction to laboratory of modern organic synthesis: Planning the synthesis of selected molecule with the use of databases and scientific literature.10
T-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by FT-IR spectroscopy.10
T-L-3Building a carbon skeleton by using palladium catalysts. The use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method ans structure analysis by MS ans NMR methods.10
30
wykłady
T-W-1Databases and scientific journals as a platform to start modern organic synthesis.1
T-W-2Principles of planning the synthesis of complex molecules. (Single and multistep one-pot reactions, domino and multicomponent reactions, etc).1
T-W-3Selected new methods for building a carbon skeleton by using palladium catalysts, organolithium and organomagensium reagents.7
T-W-4Special techniques for carrying out the reaction. (eg. at low temperature, in anhydrous solvents, microwave-assisted synthesis, solid-state synthesis, flow synthesis, green synthesis, etc.)3
T-W-5Optimization reactions, conditions and troubleshooting.1
T-W-6Application of NMR spectroscopy for solving problems in modern organic synthesis.2
15

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
laboratoria
A-L-1Participation in the laboratory classes.30
A-L-2Theoretical preparation to the laboratory classes.10
A-L-3The preparation of the written raports.10
50
wykłady
A-W-1Attendance at lectures.15
A-W-2Self study of recomended literature.8
A-W-3Examination.2
25

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Lecture with discussion.
M-2Laboratory exercises.

Sposoby oceny

KODSposób oceny
S-1Ocena podsumowująca: Continuous assessment: laboratory reports and activity.
S-2Ocena podsumowująca: Writting the exam.

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_C06_W01
The student has basic knowledge on construction of a carbon skeleton of organic compounds and various techniques of their synthesis.		ChEn_2A_W01, ChEn_2A_W02, ChEn_2A_W03, ChEn_2A_W04, ChEn_2A_W05——C-2T-W-3, T-W-4, T-W-5M-1S-2

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_C06_U01
The studen is able to plan and perform basic synthetic transformations on the basis of informations taken from databases and scientific literature and is able to analyse the products by using basic analytical methods.		ChEn_2A_U12, ChEn_2A_U03, ChEn_2A_U05, ChEn_2A_U06, ChEn_2A_U07, ChEn_2A_U08——C-3T-L-2, T-L-3, T-L-1, T-W-2, T-W-1, T-W-3, T-W-4, T-W-5, T-W-6M-2S-1
ChEn_2A_C06_U02
The studen is able to prepare the laboratory raport.		ChEn_2A_U05, ChEn_2A_U06, ChEn_2A_U07——C-3, C-2T-L-2, T-L-3, T-L-1M-2S-1

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_C06_K01
The student is aware of the importance of modern organic synthesis in life and science.		ChEn_2A_K01, ChEn_2A_K02——C-4T-W-2, T-W-1, T-W-6M-2S-1

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_C06_W01
The student has basic knowledge on construction of a carbon skeleton of organic compounds and various techniques of their synthesis.		2,0
3,0The student lists most of the modern synthetic methods applied in the construction of the carbon skeleton of organic compounds (more than 55% correct answers from the exam).
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_C06_U01
The studen is able to plan and perform basic synthetic transformations on the basis of informations taken from databases and scientific literature and is able to analyse the products by using basic analytical methods.		2,0
3,0The student prepares a plan and carries out the transformation of simple organic compounds at the basic level.
3,5
4,0
4,5
5,0
ChEn_2A_C06_U02
The studen is able to prepare the laboratory raport.		2,0
3,0The student prepares a laboratoty raport at a basic level.
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_C06_K01
The student is aware of the importance of modern organic synthesis in life and science.		2,0
3,0The student prepares a simple plan of the transformation of simple organic compounds by using at least one important modern synthetic method and one technique.
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. Pierre Vogel, Kendall N. Houk., Organic chemistry : theory, reactivity and mechanisms in modern synthesis - workbook., Wiley-VCH Verlag GMbH & C. KGaA, Weinheim, 2019
  2. Grzegorz Cholewiński, Krystyna Dzierzbicka, Dariusz Witt., Laboratory in organic chemistry, Gdańsk University of Technology Publishing House, Gdańsk, 2020
  3. John M. McIntosh., Organic chemistry : fundamentals and concepts, De Gruyter, Berlin ; Boston, 2018
  4. Paula Y. Bruice., Organic chemistry, Pearson, cop., Harlow, 2017
  5. T. W. Graham Solomons, Craig B. Fryhle., Organic chemistry, John Wiley & Sons, Hoboken, 2006

Literatura dodatkowa

  1. Koichi Tanaka., Solvent-free organic synthesis, Green Chemistry, Weinheim, 2002
  2. Raj K. Bansal, Synthetic approaches in organic chemistry, Jones and Bartlett Publ., Boston, 1998

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Regulations and safety rules in the laboratory of organic chemistry. Basic and advanced laboratory equipment. Principles of laboratory raport preparation. Introduction to laboratory of modern organic synthesis: Planning the synthesis of selected molecule with the use of databases and scientific literature.10
T-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by FT-IR spectroscopy.10
T-L-3Building a carbon skeleton by using palladium catalysts. The use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method ans structure analysis by MS ans NMR methods.10
30

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Databases and scientific journals as a platform to start modern organic synthesis.1
T-W-2Principles of planning the synthesis of complex molecules. (Single and multistep one-pot reactions, domino and multicomponent reactions, etc).1
T-W-3Selected new methods for building a carbon skeleton by using palladium catalysts, organolithium and organomagensium reagents.7
T-W-4Special techniques for carrying out the reaction. (eg. at low temperature, in anhydrous solvents, microwave-assisted synthesis, solid-state synthesis, flow synthesis, green synthesis, etc.)3
T-W-5Optimization reactions, conditions and troubleshooting.1
T-W-6Application of NMR spectroscopy for solving problems in modern organic synthesis.2
15

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1Participation in the laboratory classes.30
A-L-2Theoretical preparation to the laboratory classes.10
A-L-3The preparation of the written raports.10
50
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Attendance at lectures.15
A-W-2Self study of recomended literature.8
A-W-3Examination.2
25
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_C06_W01The student has basic knowledge on construction of a carbon skeleton of organic compounds and various techniques of their synthesis.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_W01Graduate has in-depth knowledge in the field of chemical processes, including appropriate selection of materials, raw materials, methods, techniques, equipment and devices for the implementation of chemical and biochemical processes and characterization of the raw materials and products obtained.
ChEn_2A_W02Graduate has extended and deep knowledge necessary for planning, designing and scaling-up of technological industrial processes as well as planning experiments and elaborating the results of experimental research.
ChEn_2A_W03Graduate has deep theoretical background related to catalysis and alternative and enhanced techniques in chemical and biochemical processes as well as instrumental analytical methods applied in chemical engineering.
ChEn_2A_W04Graduate has broadened and deep knowledge about the modern and green chemical and material technologies, including advanced materials and nanomaterials technologies as well as current trends in the development of chemical industrial processes.
ChEn_2A_W05Graduate has expanded knowledge in the field of environmental protection and sustainable chemical engineering, including environmental risks and dilemmas related to the implementation of industrial chemical processes as well as knows the rules of occupational health and safety.
Cel przedmiotuC-2The student knows the basic methods for construction of a carbon skeleton of organic compounds and knows the various techniques of their synthesis.
Treści programoweT-W-3Selected new methods for building a carbon skeleton by using palladium catalysts, organolithium and organomagensium reagents.
T-W-4Special techniques for carrying out the reaction. (eg. at low temperature, in anhydrous solvents, microwave-assisted synthesis, solid-state synthesis, flow synthesis, green synthesis, etc.)
T-W-5Optimization reactions, conditions and troubleshooting.
Metody nauczaniaM-1Lecture with discussion.
Sposób ocenyS-2Ocena podsumowująca: Writting the exam.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0The student lists most of the modern synthetic methods applied in the construction of the carbon skeleton of organic compounds (more than 55% correct answers from the exam).
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_C06_U01The studen is able to plan and perform basic synthetic transformations on the basis of informations taken from databases and scientific literature and is able to analyse the products by using basic analytical methods.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_U12Graduate is able to independently plan and implement his own lifelong learning and to guide others in this area.
ChEn_2A_U03Graduate is able to use broadened and deep knowledge about the modern and green chemical and material technologies as well as current trends in the development of chemical industrial processes.
ChEn_2A_U05Graduate is able to make and verify hypotheses related to simple research problems.
ChEn_2A_U06Graduate is able to analyse and solve complex problems related to chemical technology and process engineering on the basis of specialist knowledge, bibliographic resources, databases and other sources.
ChEn_2A_U07Graduate has the ability to acquire and critically evaluate information from bibliographic resources, databases and other sources and to use them in a creative way to interpret and present selected information, opinions and reports.
ChEn_2A_U08Graduate is able to apply the principles of occupational health and safety in the laboratory.
Cel przedmiotuC-3The student demonstrates the ability to conduct the basic modern organic chemistry experiments and to analyze data and results by standard analytical methods on a basic level.
Treści programoweT-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by FT-IR spectroscopy.
T-L-3Building a carbon skeleton by using palladium catalysts. The use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method ans structure analysis by MS ans NMR methods.
T-L-1Regulations and safety rules in the laboratory of organic chemistry. Basic and advanced laboratory equipment. Principles of laboratory raport preparation. Introduction to laboratory of modern organic synthesis: Planning the synthesis of selected molecule with the use of databases and scientific literature.
T-W-2Principles of planning the synthesis of complex molecules. (Single and multistep one-pot reactions, domino and multicomponent reactions, etc).
T-W-1Databases and scientific journals as a platform to start modern organic synthesis.
T-W-3Selected new methods for building a carbon skeleton by using palladium catalysts, organolithium and organomagensium reagents.
T-W-4Special techniques for carrying out the reaction. (eg. at low temperature, in anhydrous solvents, microwave-assisted synthesis, solid-state synthesis, flow synthesis, green synthesis, etc.)
T-W-5Optimization reactions, conditions and troubleshooting.
T-W-6Application of NMR spectroscopy for solving problems in modern organic synthesis.
Metody nauczaniaM-2Laboratory exercises.
Sposób ocenyS-1Ocena podsumowująca: Continuous assessment: laboratory reports and activity.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0The student prepares a plan and carries out the transformation of simple organic compounds at the basic level.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_C06_U02The studen is able to prepare the laboratory raport.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_U05Graduate is able to make and verify hypotheses related to simple research problems.
ChEn_2A_U06Graduate is able to analyse and solve complex problems related to chemical technology and process engineering on the basis of specialist knowledge, bibliographic resources, databases and other sources.
ChEn_2A_U07Graduate has the ability to acquire and critically evaluate information from bibliographic resources, databases and other sources and to use them in a creative way to interpret and present selected information, opinions and reports.
Cel przedmiotuC-3The student demonstrates the ability to conduct the basic modern organic chemistry experiments and to analyze data and results by standard analytical methods on a basic level.
C-2The student knows the basic methods for construction of a carbon skeleton of organic compounds and knows the various techniques of their synthesis.
Treści programoweT-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by FT-IR spectroscopy.
T-L-3Building a carbon skeleton by using palladium catalysts. The use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method ans structure analysis by MS ans NMR methods.
T-L-1Regulations and safety rules in the laboratory of organic chemistry. Basic and advanced laboratory equipment. Principles of laboratory raport preparation. Introduction to laboratory of modern organic synthesis: Planning the synthesis of selected molecule with the use of databases and scientific literature.
Metody nauczaniaM-2Laboratory exercises.
Sposób ocenyS-1Ocena podsumowująca: Continuous assessment: laboratory reports and activity.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0The student prepares a laboratoty raport at a basic level.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_C06_K01The student is aware of the importance of modern organic synthesis in life and science.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_K01Graduate is ready to critical assessment of own knowledge and received information and understands the need for lifelong learning and professional development.
ChEn_2A_K02Graduate is aware of the importance of knowledge in solving of cognitive and practical problems and is ready to consult experts in the case of difficult problems.
Cel przedmiotuC-4The student is aware of the importance of the knowledge acquired within the subject for developement of science and for impovement of the quality of life.
Treści programoweT-W-2Principles of planning the synthesis of complex molecules. (Single and multistep one-pot reactions, domino and multicomponent reactions, etc).
T-W-1Databases and scientific journals as a platform to start modern organic synthesis.
T-W-6Application of NMR spectroscopy for solving problems in modern organic synthesis.
Metody nauczaniaM-2Laboratory exercises.
Sposób ocenyS-1Ocena podsumowująca: Continuous assessment: laboratory reports and activity.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0The student prepares a simple plan of the transformation of simple organic compounds by using at least one important modern synthetic method and one technique.
3,5
4,0
4,5
5,0